diethyl 1-(6-(benzyloxy)benzo[d][1,3]dioxol-5-yl)-4-hydroxy-6,7-dimethoxynaphthalene-2,3-dicarboxylate

Base Information

Chemical Name:diethyl 1-(6-(benzyloxy)benzo[d][1,3]dioxol-5-yl)-4-hydroxy-6,7-dimethoxynaphthalene-2,3-dicarboxylate
CAS No.:1394124-90-3
Molecular Formula:C₃₂H₃₀O₁₀
Molecular Weight:574.584
Hs Code.:

Synonyms:diethyl 1-(6-(benzyloxy)benzo[d][1,3]dioxol-5-yl)-4-hydroxy-6,7-dimethoxynaphthalene-2,3-dicarboxylate

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Chemical Property of diethyl 1-(6-(benzyloxy)benzo[d][1,3]dioxol-5-yl)-4-hydroxy-6,7-dimethoxynaphthalene-2,3-dicarboxylate

Chemical Property:

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Technology Process of diethyl 1-(6-(benzyloxy)benzo[d][1,3]dioxol-5-yl)-4-hydroxy-6,7-dimethoxynaphthalene-2,3-dicarboxylate

There total 1 articles about diethyl 1-(6-(benzyloxy)benzo[d][1,3]dioxol-5-yl)-4-hydroxy-6,7-dimethoxynaphthalene-2,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1394124-89-0
((2-(1,3-dioxolan-2-yl)-4,5-dimethoxyphenyl)-(6-benzyloxy)-benzo[d][1,3]dioxol-5-yl)methanol

: 762-21-0
acetylenedicarboxylic acid diethyl ester

: 1394124-90-3
diethyl 1-(6-(benzyloxy)benzo[d][1,3]dioxol-5-yl)-4-hydroxy-6,7-dimethoxynaphthalene-2,3-dicarboxylate

Guidance literature:: With acetic acid; In dichloromethane; for 1h;
DOI:10.1080/10286020.2011.653561

Reference yield: 97.7%

: 1394124-90-3
diethyl 1-(6-(benzyloxy)benzo[d][1,3]dioxol-5-yl)-4-hydroxy-6,7-dimethoxynaphthalene-2,3-dicarboxylate

: 1394124-91-4
6'-benzyloxydiphyllin

Guidance literature:: diethyl 1-(6-(benzyloxy)benzo[d][1,3]dioxol-5-yl)-4-hydroxy-6,7-dimethoxynaphthalene-2,3-dicarboxylate; With sodium tetrahydroborate; In tetrahydrofuran; for 3h; Reflux;

With hydrogenchloride; In tetrahydrofuran; at 20 ℃; for 1h; pH=2 - 3;
DOI:10.1080/10286020.2011.653561

Reference yield:

: 1394124-90-3
diethyl 1-(6-(benzyloxy)benzo[d][1,3]dioxol-5-yl)-4-hydroxy-6,7-dimethoxynaphthalene-2,3-dicarboxylate

: 1394124-92-5
6'-benzyloxyjusticidin A

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / tetrahydrofuran / 3 h / Reflux

1.2: 1 h / 20 °C / pH 2 - 3

2.1: potassium carbonate / acetone / 1 h / Reflux

With sodium tetrahydroborate; potassium carbonate; In tetrahydrofuran; acetone;
DOI:10.1080/10286020.2011.653561