2,2',3,3',4,4'-hexa-O-benzoyl-6,6'-bis-O-((trifluoromethyl)sulfonyl)-α,α'-trehalose

Base Information

• Chemical Name: 2,2',3,3',4,4'-hexa-O-benzoyl-6,6'-bis-O-((trifluoromethyl)sulfonyl)-α,α'-trehalose
• CAS No.: 142386-47-8
• Molecular Formula: C₅₆H₄₄F₆O₂₁S₂
• Molecular Weight: 1231.08

Synonyms:2,2',3,3',4,4'-hexa-O-benzoyl-6,6'-bis-O-((trifluoromethyl)sulfonyl)-α,α'-trehalose

Chemical Property of 2,2',3,3',4,4'-hexa-O-benzoyl-6,6'-bis-O-((trifluoromethyl)sulfonyl)-α,α'-trehalose

Chemical Property:

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Technology Process of 2,2',3,3',4,4'-hexa-O-benzoyl-6,6'-bis-O-((trifluoromethyl)sulfonyl)-α,α'-trehalose

There total 1 articles about 2,2',3,3',4,4'-hexa-O-benzoyl-6,6'-bis-O-((trifluoromethyl)sulfonyl)-α,α'-trehalose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

trifluoromethylsulfonic anhydride (358-23-6) + 2,3,4,2',3',4'-hexakis-O-benzoyl-α,α-D-trehalose (142386-46-7) → 2,2',3,3',4,4'-hexa-O-benzoyl-6,6'-bis-O-((trifluoromethyl)sulfonyl)-α,α'-trehalose (142386-47-8)

Guidance literature:

With pyridine; In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1016/S0008-6215(99)00069-5

Reference yield: 87.0%

potassium cyanide (151-50-8) + 2,2',3,3',4,4'-hexa-O-benzoyl-6,6'-bis-O-((trifluoromethyl)sulfonyl)-α,α'-trehalose (142386-47-8) → 2,3,4,2',3',4'-hexa-O-benzoyl-6,6'-dicyano-6,6'-dideoxy-α,α-trehalose (243132-04-9)

Guidance literature:

In water; acetonitrile; at 20 ℃; for 24h;

DOI:10.1016/S0008-6215(99)00069-5

Reference yield: 71.0%

hexan-1-amine (111-26-2) + 2,2',3,3',4,4'-hexa-O-benzoyl-6,6'-bis-O-((trifluoromethyl)sulfonyl)-α,α'-trehalose (142386-47-8) → 2,3,4,2',3',4'-hexa-O-benzoyl-6,6'-dideoxy-6,6'-bis(1-hexylamino)-α,α-trehalose

Guidance literature:

In dichloromethane; at 20 ℃; for 48h;

DOI:10.1016/S0008-6215(01)00288-9

upstream raw materials:

trifluoromethylsulfonic anhydride

2,3,4,2',3',4'-hexakis-O-benzoyl-α,α-D-trehalose

Downstream raw materials:

C₁₃₈H₁₁₆O₃₄

C₆₉H₅₈O₁₇

C₁₂₈H₁₀₀O₃₄

(R)-2,3,4,2',3',4'-hexa-O-benzoyl-6,6'-dideoxy-6,6'-bis[1-(hydroxymethyl)propylamino]-α,α-trehalose

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