N-cyclopentyl-6-nitro-N-<(4-nitrophenoxy)propyl>-2-quinolinemethanamine

Base Information

Chemical Name:N-cyclopentyl-6-nitro-N-<(4-nitrophenoxy)propyl>-2-quinolinemethanamine
CAS No.:137898-56-7
Molecular Formula:C₂₄H₂₆N₄O₅
Molecular Weight:450.494
Hs Code.:

Synonyms:N-cyclopentyl-6-nitro-N-<(4-nitrophenoxy)propyl>-2-quinolinemethanamine

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Chemical Property of N-cyclopentyl-6-nitro-N-<(4-nitrophenoxy)propyl>-2-quinolinemethanamine

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Technology Process of N-cyclopentyl-6-nitro-N-<(4-nitrophenoxy)propyl>-2-quinolinemethanamine

There total 5 articles about N-cyclopentyl-6-nitro-N-<(4-nitrophenoxy)propyl>-2-quinolinemethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 76253-77-5
2-(chloromethyl)-6-nitroquinoline

: 137898-53-4
N-<3-(4-nitrophenoxy)propyl>cyclopentylamine

: 137898-56-7
N-cyclopentyl-6-nitro-N-<(4-nitrophenoxy)propyl>-2-quinolinemethanamine

Guidance literature:: With potassium carbonate; sodium iodide; In ethanol; acetonitrile; at 60 ℃; for 24h;
DOI:10.1021/jm00115a010

Reference yield:

: 79096-54-1
1-(3-Chloropropoxy)-4-nitrobenzene

: 137898-56-7
N-cyclopentyl-6-nitro-N-<(4-nitrophenoxy)propyl>-2-quinolinemethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃, NaI / ethanol; acetonitrile / 24 h / 60 °C

2: 62 percent / K₂CO₃, NaI / ethanol; acetonitrile / 24 h / 60 °C

With potassium carbonate; sodium iodide; In ethanol; acetonitrile;
DOI:10.1021/jm00115a010

Reference yield:

: 76253-89-9
2-methyl-6-nitroquinoline N-oxide

: 137898-56-7
N-cyclopentyl-6-nitro-N-<(4-nitrophenoxy)propyl>-2-quinolinemethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / p-toluenesulfonyl chloride / 1,2-dichloro-ethane / 1.) 100 deg C, 24 h, 2.) RT, 48 h

2: 62 percent / K₂CO₃, NaI / ethanol; acetonitrile / 24 h / 60 °C

With potassium carbonate; p-toluenesulfonyl chloride; sodium iodide; In ethanol; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/jm00115a010