C₆H₄⁽²⁾HClO

Base Information

• Chemical Name: C₆H₄⁽²⁾HClO
• CAS No.: 74383-28-1
• Molecular Formula: C₆H₅ClO
• Molecular Weight: 129.55
• Mol file: 74383-28-1.mol

Synonyms:C₆H₄⁽²⁾HClO

Chemical Property of C₆H₄⁽²⁾HClO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of C₆H₄⁽²⁾HClO

There total 3 articles about C₆H₄⁽²⁾HClO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

3-monochlorophenol (108-43-0) → C6H4(2)HClO (74383-28-1)

Guidance literature:

With potassium acetate; C₄₃H₅₇ClIrN₃; deuterium hydride; In dichloromethane; at 35 ℃; for 10h; Sealed tube;

DOI:10.1021/acs.orglett.1c03685

Reference yield:

1-chloro-4-deuterio-benzene (13122-34-4) → 3-monochlorophenol (108-43-0) + C6H4(2)HClO (74383-28-1) + C6H4(2)HClO (116467-74-4) + 4-chloro-phenol (106-48-9,82344-39-6)

Guidance literature:

With ferrous perchlorate; copper(II) ion; dihydrogen peroxide; In water; acetonitrile; at 25 ℃; for 0.5h; Product distribution; further oxidants;

DOI:10.1021/ja00230a032

Reference yield:

1-chloro-4-deuterio-benzene (13122-34-4) → phenol-d1 (1003-66-3) + 3-chloro-O-deuterio-phenol (65750-22-3) + p-Chlorophenol-OD (14915-23-2) + 2-(2H)-4-chlorophenol (116467-75-5) + C6H4(2)HClO (74383-28-1) + 4-chloro-phenol (106-48-9,82344-39-6)

Guidance literature:

With triplet atomic oxygen O(³P); In various solvent(s); at 50.9 ℃; under 22.5 - 75.006 Torr; Mechanism; Product distribution; Rate constant; phenols, chlorophenols were analysed by GC-MS of their trimethylsilyl derivatives;

upstream raw materials:

1-chloro-4-deuterio-benzene

3-monochlorophenol