tert-Butyl-dimethyl-{1-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-cyclohexa-2,5-dienylmethoxy}-silane

Base Information

Chemical Name:tert-Butyl-dimethyl-{1-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-cyclohexa-2,5-dienylmethoxy}-silane
CAS No.:142389-45-5
Molecular Formula:C₁₉H₃₄O₃Si
Molecular Weight:338.563
Hs Code.:

Synonyms:tert-Butyl-dimethyl-{1-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-cyclohexa-2,5-dienylmethoxy}-silane

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Chemical Property of tert-Butyl-dimethyl-{1-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-cyclohexa-2,5-dienylmethoxy}-silane

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Technology Process of tert-Butyl-dimethyl-{1-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-cyclohexa-2,5-dienylmethoxy}-silane

There total 4 articles about tert-Butyl-dimethyl-{1-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-cyclohexa-2,5-dienylmethoxy}-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: {1-[2-(2-Methyl-[1,3]dioxolan-2-yl)-ethyl]-cyclohexa-2,5-dienyl}-methanol

: 142389-45-5
tert-Butyl-dimethyl-{1-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-cyclohexa-2,5-dienylmethoxy}-silane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)92252-4

Reference yield:

: 30889-20-4
methyl cyclohexa-2,5-diene-1-carboxylate

: 142389-45-5
tert-Butyl-dimethyl-{1-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-cyclohexa-2,5-dienylmethoxy}-silane

Guidance literature:: Multi-step reaction with 4 steps

1: 1) LDA / 1) THF, HMPA, 2) -78 deg C, 50 min

2: 93 percent / p-TsOH / benzene / Heating

3: 100 percent / LiAlH₄ / diethyl ether / 0 °C

4: 100 percent / imidazole / dimethylformamide

With 1H-imidazole; lithium aluminium tetrahydride; toluene-4-sulfonic acid; lithium diisopropyl amide; In diethyl ether; N,N-dimethyl-formamide; benzene;
DOI:10.1016/S0040-4039(00)92252-4

Reference yield:

: 142389-43-3
1-(3-Oxo-butyl)-cyclohexa-2,5-dienecarboxylic acid methyl ester

: 142389-45-5
tert-Butyl-dimethyl-{1-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl]-cyclohexa-2,5-dienylmethoxy}-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / p-TsOH / benzene / Heating

2: 100 percent / LiAlH₄ / diethyl ether / 0 °C

3: 100 percent / imidazole / dimethylformamide

With 1H-imidazole; lithium aluminium tetrahydride; toluene-4-sulfonic acid; In diethyl ether; N,N-dimethyl-formamide; benzene;
DOI:10.1016/S0040-4039(00)92252-4