4-O-benzoyl-2-bromo-2,6-dideoxy-3-O-formyl-α-D-galactopyranosyl bromide

Base Information

Chemical Name:4-O-benzoyl-2-bromo-2,6-dideoxy-3-O-formyl-α-D-galactopyranosyl bromide
CAS No.:108319-51-3
Molecular Formula:C₁₄H₁₄Br₂O₅
Molecular Weight:422.07
Hs Code.:

Synonyms:4-O-benzoyl-2-bromo-2,6-dideoxy-3-O-formyl-α-D-galactopyranosyl bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-O-benzoyl-2-bromo-2,6-dideoxy-3-O-formyl-α-D-galactopyranosyl bromide

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Technology Process of 4-O-benzoyl-2-bromo-2,6-dideoxy-3-O-formyl-α-D-galactopyranosyl bromide

There total 6 articles about 4-O-benzoyl-2-bromo-2,6-dideoxy-3-O-formyl-α-D-galactopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 3492-44-2
α,α-dibromomethyl methyl ether

: 108319-50-2
methyl 4-O-benzoyl-6-deoxy-2,3-O-isopropylidene-α-D-talopyranoside

: 108319-51-3
4-O-benzoyl-2-bromo-2,6-dideoxy-3-O-formyl-α-D-galactopyranosyl bromide

Guidance literature:: With zinc dibromide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1080/07328303.2017.1397682

Reference yield:

: 14133-63-2,14685-82-6,22932-38-3,24562-43-4,33947-10-3,42214-01-7,52572-07-3,72251-91-3,72251-92-4,72959-81-0,104846-19-7,149035-63-2
methyl 2,3-O-isopropylidene-α-D-rhamnopyranoside

: 108319-51-3
4-O-benzoyl-2-bromo-2,6-dideoxy-3-O-formyl-α-D-galactopyranosyl bromide

Guidance literature:: Multi-step reaction with 4 steps

1: 62 percent / (C₆H₅N)2Cr₂O₇, CH₃COOH / CH₂Cl₂

2: 82 percent / LiAlH₄

3: 82 percent / pyridine

4: 70 percent / Br₂CHOCH₃ / ZnBr₂

With pyridine; lithium aluminium tetrahydride; α,α-dibromomethyl methyl ether; (C₆H₅N)2Cr₂O₇; acetic acid; zinc dibromide; In dichloromethane;

Reference yield:

: 104846-19-7
methyl 6-deoxy-2,3-O-isopropylidene-α-D-talopyranoside

: 108319-51-3
4-O-benzoyl-2-bromo-2,6-dideoxy-3-O-formyl-α-D-galactopyranosyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / pyridine

2: 70 percent / Br₂CHOCH₃ / ZnBr₂

With pyridine; α,α-dibromomethyl methyl ether; zinc dibromide;