tert-butyl 2-benzyloxy-2-{1-[chloro(p-tolylsulfinyl)methyl]cyclohexyl}acetate

Base Information

Chemical Name:tert-butyl 2-benzyloxy-2-{1-[chloro(p-tolylsulfinyl)methyl]cyclohexyl}acetate
CAS No.:956904-48-6
Molecular Formula:C₂₇H₃₅ClO₄S
Molecular Weight:491.091
Hs Code.:

Synonyms:tert-butyl 2-benzyloxy-2-{1-[chloro(p-tolylsulfinyl)methyl]cyclohexyl}acetate

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Chemical Property of tert-butyl 2-benzyloxy-2-{1-[chloro(p-tolylsulfinyl)methyl]cyclohexyl}acetate

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Technology Process of tert-butyl 2-benzyloxy-2-{1-[chloro(p-tolylsulfinyl)methyl]cyclohexyl}acetate

There total 3 articles about tert-butyl 2-benzyloxy-2-{1-[chloro(p-tolylsulfinyl)methyl]cyclohexyl}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 867150-88-7
1-((R)-Chloro-cyclohexylidene-methanesulfinyl)-4-methyl-benzene

: 119620-31-4
benzyloxyacetic acid t-butyl ester

: 956904-48-6
tert-butyl 2-benzyloxy-2-{1-[chloro(p-tolylsulfinyl)methyl]cyclohexyl}acetate

Guidance literature:: benzyloxyacetic acid t-butyl ester; With lithium diisopropyl amide; In tetrahydrofuran; at -45 ℃; for 0.25h;

1-((R)-Chloro-cyclohexylidene-methanesulfinyl)-4-methyl-benzene; In tetrahydrofuran; at -45 ℃; Further stages.;
DOI:10.1016/j.tetasy.2007.07.033

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 956904-48-6
tert-butyl 2-benzyloxy-2-{1-[chloro(p-tolylsulfinyl)methyl]cyclohexyl}acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: LDA / tetrahydrofuran / 0.25 h / -45 °C

1.2: 95 percent / tetrahydrofuran / -45 °C

With lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2007.07.033

Reference yield:

: 31350-91-1
(R)-chloromethyl p-tolyl sulfoxide

: 956904-48-6
tert-butyl 2-benzyloxy-2-{1-[chloro(p-tolylsulfinyl)methyl]cyclohexyl}acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: LDA / tetrahydrofuran / 0.25 h / -45 °C

1.2: 95 percent / tetrahydrofuran / -45 °C

With lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2007.07.033