3-nitro-benzenesulfonic acid-(2,4,6-trichloro-phenyl ester)

Base Information

• Chemical Name: 3-nitro-benzenesulfonic acid-(2,4,6-trichloro-phenyl ester)
• CAS No.: 934986-59-1
• Molecular Formula: C₁₂H₆Cl₃NO₅S
• Molecular Weight: 382.608
• Mol file: 934986-59-1.mol

Synonyms:3-nitro-benzenesulfonic acid-(2,4,6-trichloro-phenyl ester)

Chemical Property of 3-nitro-benzenesulfonic acid-(2,4,6-trichloro-phenyl ester)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3-nitro-benzenesulfonic acid-(2,4,6-trichloro-phenyl ester)

There total 4 articles about 3-nitro-benzenesulfonic acid-(2,4,6-trichloro-phenyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

pyridinium paratoluene sulfonic acid (84752-61-4) + 2,4,6-Trichlorophenol (88-06-2,67471-29-8) → 3-nitro-benzenesulfonic acid-(2,4,6-trichloro-phenyl ester) (934986-59-1)

Guidance literature:

With triethylamine; In dichloromethane;

DOI:10.1039/b614604j

Reference yield:

2,4,6-trichlorophenyl benzenesulfonate (105522-47-2) → 3-nitro-benzenesulfonic acid-(2,4,6-trichloro-phenyl ester) (934986-59-1)

Guidance literature:

With nitric acid;

Reference yield:

benzenesulfonyl chloride (98-09-9) → 3-nitro-benzenesulfonic acid-(2,4,6-trichloro-phenyl ester) (934986-59-1)

Guidance literature:

Multi-step reaction with 2 steps

1: diluted KOH-solution

2: fuming nitric acid

With potassium hydroxide; nitric acid;

upstream raw materials:

2,4,6-trichlorophenyl benzenesulfonate

pyridinium paratoluene sulfonic acid

2,4,6-Trichlorophenol

benzenesulfonyl chloride

Downstream raw materials:

2,4,6-Trichlorophenol