Technology Process of C58H56N2O11
There total 5 articles about C58H56N2O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutylammomium bromide; sodium hydroxide;
In
chloroform; water;
at 50 ℃;
for 4h;
stereoselective reaction;
DOI:10.1021/ol301352v
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
3: hydrazine hydrate / tetrahydrofuran / 3 h / 20 °C
4: tetrabutylammomium bromide; sodium hydroxide / chloroform; water / 4 h / 50 °C
With
tetrabutylammomium bromide; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; chloroform; water;
DOI:10.1021/ol301352v
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrazine hydrate / tetrahydrofuran / 3 h / 20 °C
2: tetrabutylammomium bromide; sodium hydroxide / chloroform; water / 4 h / 50 °C
With
tetrabutylammomium bromide; hydrazine hydrate; sodium hydroxide;
In
tetrahydrofuran; chloroform; water;
DOI:10.1021/ol301352v
