(2E,4E)-ethyl 6-((4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-3-oxonona-4,6-dienamido)-5-methylhexa-2,4-dienoate

Base Information

• Chemical Name: (2E,4E)-ethyl 6-((4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-3-oxonona-4,6-dienamido)-5-methylhexa-2,4-dienoate
• CAS No.: 1443224-12-1
• Molecular Formula: C₂₈H₃₇NO₅
• Molecular Weight: 467.605

Synonyms:(2E,4E)-ethyl 6-((4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-3-oxonona-4,6-dienamido)-5-methylhexa-2,4-dienoate

Chemical Property of (2E,4E)-ethyl 6-((4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-3-oxonona-4,6-dienamido)-5-methylhexa-2,4-dienoate

Chemical Property:

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Technology Process of (2E,4E)-ethyl 6-((4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-3-oxonona-4,6-dienamido)-5-methylhexa-2,4-dienoate

There total 3 articles about (2E,4E)-ethyl 6-((4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-3-oxonona-4,6-dienamido)-5-methylhexa-2,4-dienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

(2E,4E)-ethyl 6-((4-methoxybenzyl)amino)-5-methylhexa-2,4-dienoate (1443224-03-0) + 6-((1E,3E)-3,5-dimethylhexa-1,3-dien-1-yl)-2,2-dimethyl-4H-1,3-dioxin-4-one (1443224-01-8) → (2E,4E)-ethyl 6-((4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-3-oxonona-4,6-dienamido)-5-methylhexa-2,4-dienoate (1443224-12-1)

Guidance literature:

With pyridinium p-toluenesulfonate; In toluene; at 110 ℃; for 3h; Inert atmosphere;

DOI:10.1021/ol401354a

Reference yield:

ethyl 6-bromo-5-methylhexa-2,4-dienoate → (2E,4E)-ethyl 6-((4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-3-oxonona-4,6-dienamido)-5-methylhexa-2,4-dienoate (1443224-12-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 0 - 23 °C / Inert atmosphere

2: pyridinium p-toluenesulfonate / toluene / 3 h / 110 °C / Inert atmosphere

With pyridinium p-toluenesulfonate; potassium carbonate; In N,N-dimethyl-formamide; toluene;

DOI:10.1021/ol401354a

Reference yield:

4-methoxy-benzylamine (2393-23-9) → (2E,4E)-ethyl 6-((4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-3-oxonona-4,6-dienamido)-5-methylhexa-2,4-dienoate (1443224-12-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 0 - 23 °C / Inert atmosphere

2: pyridinium p-toluenesulfonate / toluene / 3 h / 110 °C / Inert atmosphere

With pyridinium p-toluenesulfonate; potassium carbonate; In N,N-dimethyl-formamide; toluene;

DOI:10.1021/ol401354a

upstream raw materials:

(2E,4E)-ethyl 6-((4-methoxybenzyl)amino)-5-methylhexa-2,4-dienoate

6-((1E,3E)-3,5-dimethylhexa-1,3-dien-1-yl)-2,2-dimethyl-4H-1,3-dioxin-4-one

4-methoxy-benzylamine

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