diphenylmethyl 2-<(1-p-methoxybenzylthio)cyclopentyl>-2-<(methylthio)methylimino>acetate

Base Information

• Chemical Name: diphenylmethyl 2-<(1-p-methoxybenzylthio)cyclopentyl>-2-<(methylthio)methylimino>acetate
• CAS No.: 75996-04-2
• Molecular Formula: C₃₀H₃₃NO₃S₂
• Molecular Weight: 519.729
• Mol file: 75996-04-2.mol

Synonyms:diphenylmethyl 2-<(1-p-methoxybenzylthio)cyclopentyl>-2-<(methylthio)methylimino>acetate

Chemical Property of diphenylmethyl 2-<(1-p-methoxybenzylthio)cyclopentyl>-2-<(methylthio)methylimino>acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diphenylmethyl 2-<(1-p-methoxybenzylthio)cyclopentyl>-2-<(methylthio)methylimino>acetate

There total 5 articles about diphenylmethyl 2-<(1-p-methoxybenzylthio)cyclopentyl>-2-<(methylthio)methylimino>acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

diphenylmethyl 2-<(1-p-methoxybenzylthio)cyclopentyl>-2-(thioformamido)acetate (75996-02-0) + methyl iodide (74-88-4) → diphenylmethyl 2-<(1-p-methoxybenzylthio)cyclopentyl>-2-<(methylthio)methylimino>acetate (75996-04-2)

Guidance literature:

With potassium carbonate; In acetone; for 40h; Ambient temperature;

DOI:10.1039/P19800002228

Reference yield:

2-amino-2-(1-mercaptocyclopentyl)acetic acid hydrochloride (43180-45-6) → diphenylmethyl 2-<(1-p-methoxybenzylthio)cyclopentyl>-2-<(methylthio)methylimino>acetate (75996-04-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 87 percent / sodium / liquid ammonia / 0.5 h

2: 1.) hydrogen sulphide, 2.) triethylamine / 1.) chloroform, 15 min, 2.) 16 h

3: 50.0 g / acetone

4: 96 percent / potassium carbonate / acetone / 40 h / Ambient temperature

With hydrogen sulfide; sodium; potassium carbonate; triethylamine; In ammonia; acetone;

DOI:10.1039/P19800002228

Reference yield:

2-amino-2-<(1-p-methoxybenzylthio)cyclopentyl>acetic acid (75996-00-8) → diphenylmethyl 2-<(1-p-methoxybenzylthio)cyclopentyl>-2-<(methylthio)methylimino>acetate (75996-04-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) hydrogen sulphide, 2.) triethylamine / 1.) chloroform, 15 min, 2.) 16 h

2: 50.0 g / acetone

3: 96 percent / potassium carbonate / acetone / 40 h / Ambient temperature

With hydrogen sulfide; potassium carbonate; triethylamine; In acetone;

DOI:10.1039/P19800002228

upstream raw materials:

diphenylmethyl 2-<(1-p-methoxybenzylthio)cyclopentyl>-2-(thioformamido)acetate

methyl iodide

2-amino-2-(1-mercaptocyclopentyl)acetic acid hydrochloride

2-amino-2-<(1-p-methoxybenzylthio)cyclopentyl>acetic acid