(2E/Z,4E)-2,3-dimethyl-5-(2’,6’,6’-trimethylcyclohex-1’-en-1’-yl)penta-2,4-dienenitrile

Base Information

• Chemical Name: (2E/Z,4E)-2,3-dimethyl-5-(2’,6’,6’-trimethylcyclohex-1’-en-1’-yl)penta-2,4-dienenitrile
• CAS No.: 1377907-00-0
• Molecular Formula: C₁₆H₂₃N
• Molecular Weight: 229.365

Synonyms:(2E/Z,4E)-2,3-dimethyl-5-(2’,6’,6’-trimethylcyclohex-1’-en-1’-yl)penta-2,4-dienenitrile

Chemical Property of (2E/Z,4E)-2,3-dimethyl-5-(2’,6’,6’-trimethylcyclohex-1’-en-1’-yl)penta-2,4-dienenitrile

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Technology Process of (2E/Z,4E)-2,3-dimethyl-5-(2’,6’,6’-trimethylcyclohex-1’-en-1’-yl)penta-2,4-dienenitrile

There total 1 articles about (2E/Z,4E)-2,3-dimethyl-5-(2’,6’,6’-trimethylcyclohex-1’-en-1’-yl)penta-2,4-dienenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

diethyl (1-cyanoethyl)phosphonate (29668-61-9) + alpha-ionone (127-41-3,6901-97-9,14398-36-8,24190-29-2,30685-95-1,31798-12-6,52340-45-1,67529-94-6,67529-95-7) → (2E/Z,4E)-2,3-dimethyl-5-(2’,6’,6’-trimethylcyclohex-1’-en-1’-yl)penta-2,4-dienenitrile (1377907-00-0)

Guidance literature:

diethyl (1-cyanoethyl)phosphonate; With n-butyllithium; In tetrahydrofuran; hexane; cyclohexane; at -78 ℃; for 0.5h; Inert atmosphere;

alpha-ionone; In tetrahydrofuran; hexane; cyclohexane; at -78 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja3007929

Reference yield: 91.0%

(2E/Z,4E)-2,3-dimethyl-5-(2’,6’,6’-trimethylcyclohex-1’-en-1’-yl)penta-2,4-dienenitrile (1377907-00-0) → 2,3-dimethyl-5-(2',6',6'-trimethyl-1'-cyclohexen-1'-yl)-2,4-pentadienal

Guidance literature:

With diisobutylaluminium hydride; In hexane; at -50 ℃; for 0.583333h; Inert atmosphere;

DOI:10.1021/ja3007929

Reference yield: 28.0%

(2E/Z,4E)-2,3-dimethyl-5-(2’,6’,6’-trimethylcyclohex-1’-en-1’-yl)penta-2,4-dienenitrile (1377907-00-0) → (2E,4E)-2,3-dimethyl-5-(2’,6’,6’-trimethylcyclohex-1’-en-1’-yl)penta-2,4-dienal (67310-08-1)

Guidance literature:

With diisobutylaluminium hydride; In hexane; chloroform; at -50 ℃; Inert atmosphere;

DOI:10.1021/ja4121814

upstream raw materials:

diethyl (1-cyanoethyl)phosphonate

alpha-ionone

Downstream raw materials:

(2E,4E)-2,3-dimethyl-5-(2’,6’,6’-trimethylcyclohex-1’-en-1’-yl)penta-2,4-dienal

all-trans-10,14-dimethyl-retinal

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