P--P-methyldibenzylphospholium trifluoromethanesulfonate

Base Information

Chemical Name:P--P-methyldibenzylphospholium trifluoromethanesulfonate
CAS No.:121192-54-9
Molecular Formula:CF₃O₃S*C₂₄H₃₀O₃P
Molecular Weight:546.545
Hs Code.:

P-<erythro-(1-Carbethoxy-2-cyclohexyl-2-hydroxyethyl)>-P-methyldibenzylphospholium trifluoromethanesulfonate

Synonyms:P--P-methyldibenzylphospholium trifluoromethanesulfonate

Suppliers and Price of P--P-methyldibenzylphospholium trifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of P--P-methyldibenzylphospholium trifluoromethanesulfonate

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Technology Process of P--P-methyldibenzylphospholium trifluoromethanesulfonate

There total 3 articles about P--P-methyldibenzylphospholium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121192-43-6
P-(Carbethoxymethyl)dibenzophosphole

: 121192-54-9
P--P-methyldibenzylphospholium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, diisopropylamine / 1.) THF, hexane, -78 deg C, 15 min; 2.) 15 min

2: hexane; diethyl ether; CH₂Cl₂

With n-butyllithium; diisopropylamine; In diethyl ether; hexane; dichloromethane;
DOI:10.1021/ja00197a055

Reference yield:

: 244-87-1
5H-benzo[b]phosphindole

: 121192-54-9
P--P-methyldibenzylphospholium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 14 percent / Na₂CO₃ / 24 h

2: 1.) n-BuLi, diisopropylamine / 1.) THF, hexane, -78 deg C, 15 min; 2.) 15 min

3: hexane; diethyl ether; CH₂Cl₂

With n-butyllithium; sodium carbonate; diisopropylamine; In diethyl ether; hexane; dichloromethane;
DOI:10.1021/ja00197a055