3-[4,6-bis-cyclopropylamino-1,3,5-triazin-2-yl-oxy]-4-methoxybenzaldehyde

Base Information

• Chemical Name: 3-[4,6-bis-cyclopropylamino-1,3,5-triazin-2-yl-oxy]-4-methoxybenzaldehyde
• CAS No.: 1321610-87-0
• Molecular Formula: C₁₇H₁₉N₅O₃
• Molecular Weight: 341.37

Synonyms:3-[4,6-bis-cyclopropylamino-1,3,5-triazin-2-yl-oxy]-4-methoxybenzaldehyde

Chemical Property of 3-[4,6-bis-cyclopropylamino-1,3,5-triazin-2-yl-oxy]-4-methoxybenzaldehyde

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Technology Process of 3-[4,6-bis-cyclopropylamino-1,3,5-triazin-2-yl-oxy]-4-methoxybenzaldehyde

There total 1 articles about 3-[4,6-bis-cyclopropylamino-1,3,5-triazin-2-yl-oxy]-4-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.1%

isovanillin (621-59-0) + 6-chloro-N2,N4-dicyclopropyl-1,3,5-triazine-2,4-diamine (22936-82-9) → 3-[4,6-bis-cyclopropylamino-1,3,5-triazin-2-yl-oxy]-4-methoxybenzaldehyde (1321610-87-0)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 6h;

Reference yield: 67.1%

indole (120-72-9) + 3-[4,6-bis-cyclopropylamino-1,3,5-triazin-2-yl-oxy]-4-methoxybenzaldehyde (1321610-87-0) → 2,2'-[2,2'-3-(4,6-bis-cyclopropylamino)-1,3,5-triazin-2-yl-oxy-4-methoxyphenyl]methylene-bis-1H-indole (1321610-83-6)

Guidance literature:

With 1,3,5-trichloro-2,4,6-triazine; In acetonitrile; at 60 ℃; for 8h;

Reference yield: 61.0%

indole-3-acetic acid (87-51-4) + 3-[4,6-bis-cyclopropylamino-1,3,5-triazin-2-yl-oxy]-4-methoxybenzaldehyde (1321610-87-0) → 2,2'-[2,2'-3-(4,6-bis-cyclopropylamino)-1,3,5-triazin-2-yl-oxy-4-methoxyphenyl]methylene-bis-(1H-indole-3,3-diyl)diacetic acid (1321610-85-8)

Guidance literature:

With zirconium(IV) chloride; In acetonitrile; at 60 ℃; for 8h;

DOI:10.1039/c5ra11495k

upstream raw materials:

isovanillin

6-chloro-N²,N⁴-dicyclopropyl-1,3,5-triazine-2,4-diamine

Downstream raw materials:

2,2'-[2,2'-3-(4,6-bis-cyclopropylamino)-1,3,5-triazin-2-yl-oxy-4-methoxyphenyl]methylene-bis-(1H-indole-3,3-diyl)diacetic acid

2,2'-[2,2'-3-(4,6-bis-cyclopropylamino)-1,3,5-triazin-2-yl-oxy-4-methoxyphenyl]methylene-bis-1H-indole

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