(S)-N-(1-phenylethyl)-N-3-(ethoxycarbonyl-2(E)-propen-1-yl)amine hydrobromide

Base Information

Chemical Name:(S)-N-(1-phenylethyl)-N-3-(ethoxycarbonyl-2(E)-propen-1-yl)amine hydrobromide
CAS No.:114948-66-2
Molecular Formula:BrH*C₁₄H₁₉NO₂
Molecular Weight:314.222
Hs Code.:

Synonyms:(S)-N-(1-phenylethyl)-N-3-(ethoxycarbonyl-2(E)-propen-1-yl)amine hydrobromide

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Chemical Property of (S)-N-(1-phenylethyl)-N-3-(ethoxycarbonyl-2(E)-propen-1-yl)amine hydrobromide

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Technology Process of (S)-N-(1-phenylethyl)-N-3-(ethoxycarbonyl-2(E)-propen-1-yl)amine hydrobromide

There total 1 articles about (S)-N-(1-phenylethyl)-N-3-(ethoxycarbonyl-2(E)-propen-1-yl)amine hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 37746-78-4
4-bromo-trans-crotonic acid ethyl ester

: 2627-86-3
(S)-1-phenyl-ethylamine

: 114948-66-2
(S)-N-(1-phenylethyl)-N-3-(ethoxycarbonyl-2(E)-propen-1-yl)amine hydrobromide

Guidance literature:: 1) 0 deg C, 1 h, 2) room temperature, 3 h;
DOI:10.1016/S0040-4020(01)90313-8

Reference yield: 90.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 114948-66-2
(S)-N-(1-phenylethyl)-N-3-(ethoxycarbonyl-2(E)-propen-1-yl)amine hydrobromide

: 114948-67-3
(S)-N-(1-phenylethyl)-N-3-(ethoxycarbonyl-2(E)-propen-1-yl)-N-(benzyloxycarbonyl)amine

Guidance literature:: With sodium hydrogencarbonate; In water; acetone; for 1h;
DOI:10.1016/S0040-4020(01)90313-8

Reference yield:

: 114948-66-2
(S)-N-(1-phenylethyl)-N-3-(ethoxycarbonyl-2(E)-propen-1-yl)amine hydrobromide

: 114948-73-1
(5S)-3-<(1S)-phenylethyl>-5-(carboxymethyl)oxazolidin-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / NaHCO₃ / H₂O; acetone / 1 h

2: 47 percent / I₂ / CHCl₃ / 5 h / Ambient temperature

3: tri-n-butyltinhydride / benzene / 5 h / Heating

4: 6 M HCl / acetone / 3 h / Heating

With hydrogenchloride; iodine; tri-n-butyl-tin hydride; sodium hydrogencarbonate; In chloroform; water; acetone; benzene;
DOI:10.1016/S0040-4020(01)90313-8