sodium (S)-2-(4-(4-((((3Z,6Z)-6-benzylidene-3-((5-(tert-butyl)-1H-imidazol-4-yl)methylene)-5-oxo-3,4,5,6-tetrahydropyrazin-2-yl)oxy)methoxy)-4-oxobutyl)-1H-1,2,3-triazol-1-yl)-3-hydroxypropanoate

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Chemical Name:sodium (S)-2-(4-(4-((((3Z,6Z)-6-benzylidene-3-((5-(tert-butyl)-1H-imidazol-4-yl)methylene)-5-oxo-3,4,5,6-tetrahydropyrazin-2-yl)oxy)methoxy)-4-oxobutyl)-1H-1,2,3-triazol-1-yl)-3-hydroxypropanoate
CAS No.:1360790-10-8
Molecular Formula:C₂₉H₃₂N₇O₇*Na
Molecular Weight:613.606
Hs Code.:

sodium (S)-2-(4-(4-((((3Z,6Z)-6-benzylidene-3-((5-(tert-butyl)-1H-imidazol-4-yl)methylene)-5-oxo-3,4,5,6-tetrahydropyrazin-2-yl)oxy)methoxy)-4-oxobutyl)-1H-1,2,3-triazol-1-yl)-3-hydroxypropanoate

Synonyms:sodium (S)-2-(4-(4-((((3Z,6Z)-6-benzylidene-3-((5-(tert-butyl)-1H-imidazol-4-yl)methylene)-5-oxo-3,4,5,6-tetrahydropyrazin-2-yl)oxy)methoxy)-4-oxobutyl)-1H-1,2,3-triazol-1-yl)-3-hydroxypropanoate

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Chemical Property of sodium (S)-2-(4-(4-((((3Z,6Z)-6-benzylidene-3-((5-(tert-butyl)-1H-imidazol-4-yl)methylene)-5-oxo-3,4,5,6-tetrahydropyrazin-2-yl)oxy)methoxy)-4-oxobutyl)-1H-1,2,3-triazol-1-yl)-3-hydroxypropanoate

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Technology Process of sodium (S)-2-(4-(4-((((3Z,6Z)-6-benzylidene-3-((5-(tert-butyl)-1H-imidazol-4-yl)methylene)-5-oxo-3,4,5,6-tetrahydropyrazin-2-yl)oxy)methoxy)-4-oxobutyl)-1H-1,2,3-triazol-1-yl)-3-hydroxypropanoate

There total 4 articles about sodium (S)-2-(4-(4-((((3Z,6Z)-6-benzylidene-3-((5-(tert-butyl)-1H-imidazol-4-yl)methylene)-5-oxo-3,4,5,6-tetrahydropyrazin-2-yl)oxy)methoxy)-4-oxobutyl)-1H-1,2,3-triazol-1-yl)-3-hydroxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1360790-07-3
chloromethyl hex-5-ynoate

: 1360790-10-8
sodium (S)-2-(4-(4-((((3Z,6Z)-6-benzylidene-3-((5-(tert-butyl)-1H-imidazol-4-yl)methylene)-5-oxo-3,4,5,6-tetrahydropyrazin-2-yl)oxy)methoxy)-4-oxobutyl)-1H-1,2,3-triazol-1-yl)-3-hydroxypropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 0.25 h / 50 °C / Microwave irradiation

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; N,N-dimethyl-formamide; tert-butyl alcohol / 0.17 h / 50 °C / Microwave irradiation

3: ion exchange resin DIAION WK₁₁ / water; acetonitrile

With copper(ll) sulfate pentahydrate; caesium carbonate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 2: Huisgen reaction;
DOI:10.1002/chem.201102293

Reference yield:

: 714272-27-2
(3Z,6Z)-3-[[5-(1,1-dimethylethyl)-1H-imidazol-4-yl]methylene]-6-(phenylmethylene)piperazine-2,5-dione

: 1360790-10-8
sodium (S)-2-(4-(4-((((3Z,6Z)-6-benzylidene-3-((5-(tert-butyl)-1H-imidazol-4-yl)methylene)-5-oxo-3,4,5,6-tetrahydropyrazin-2-yl)oxy)methoxy)-4-oxobutyl)-1H-1,2,3-triazol-1-yl)-3-hydroxypropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 0.25 h / 50 °C / Microwave irradiation

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; N,N-dimethyl-formamide; tert-butyl alcohol / 0.17 h / 50 °C / Microwave irradiation

3: ion exchange resin DIAION WK₁₁ / water; acetonitrile

With copper(ll) sulfate pentahydrate; caesium carbonate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 2: Huisgen reaction;
DOI:10.1002/chem.201102293

Reference yield:

: 53293-00-8
hex-5-ynoic acid

: 1360790-10-8
sodium (S)-2-(4-(4-((((3Z,6Z)-6-benzylidene-3-((5-(tert-butyl)-1H-imidazol-4-yl)methylene)-5-oxo-3,4,5,6-tetrahydropyrazin-2-yl)oxy)methoxy)-4-oxobutyl)-1H-1,2,3-triazol-1-yl)-3-hydroxypropanoate

Guidance literature:: Multi-step reaction with 4 steps

1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate / dichloromethane; water / 1 h / 20 °C

2: caesium carbonate / N,N-dimethyl-formamide / 0.25 h / 50 °C / Microwave irradiation

3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; N,N-dimethyl-formamide; tert-butyl alcohol / 0.17 h / 50 °C / Microwave irradiation

4: ion exchange resin DIAION WK₁₁ / water; acetonitrile

With copper(ll) sulfate pentahydrate; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; caesium carbonate; sodium L-ascorbate; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 3: Huisgen reaction;
DOI:10.1002/chem.201102293