1,1-bis(4-fluorophenyl)-3,3-bis(4-methoxyphenyl)-1,2,5,7-tetrahydro-6-oxacyclopenta[cd]phenalene

Base Information

Chemical Name:1,1-bis(4-fluorophenyl)-3,3-bis(4-methoxyphenyl)-1,2,5,7-tetrahydro-6-oxacyclopenta[cd]phenalene
CAS No.:1642809-30-0
Molecular Formula:C₄₀H₃₀F₂O₃
Molecular Weight:596.673
Hs Code.:

Synonyms:1,1-bis(4-fluorophenyl)-3,3-bis(4-methoxyphenyl)-1,2,5,7-tetrahydro-6-oxacyclopenta[cd]phenalene

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Chemical Property of 1,1-bis(4-fluorophenyl)-3,3-bis(4-methoxyphenyl)-1,2,5,7-tetrahydro-6-oxacyclopenta[cd]phenalene

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Technology Process of 1,1-bis(4-fluorophenyl)-3,3-bis(4-methoxyphenyl)-1,2,5,7-tetrahydro-6-oxacyclopenta[cd]phenalene

There total 4 articles about 1,1-bis(4-fluorophenyl)-3,3-bis(4-methoxyphenyl)-1,2,5,7-tetrahydro-6-oxacyclopenta[cd]phenalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: C₄₀H₃₂F₂O₄

: 1642809-30-0
1,1-bis(4-fluorophenyl)-3,3-bis(4-methoxyphenyl)-1,2,5,7-tetrahydro-6-oxacyclopenta[cd]phenalene

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 23 ℃; for 17h;
DOI:10.1246/cl.130872

Reference yield:

: 90-96-0
bis(p-methoxyphenyl)methanone

: 1642809-30-0
1,1-bis(4-fluorophenyl)-3,3-bis(4-methoxyphenyl)-1,2,5,7-tetrahydro-6-oxacyclopenta[cd]phenalene

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium / tetrahydrofuran; hexane / Flow reactor

2: n-butyllithium / tetrahydrofuran; hexane / Flow reactor

3: trifluoroacetic acid / dichloromethane / 17 h / 23 °C

With n-butyllithium; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1246/cl.130872

Reference yield:

: 19190-91-1
5,6-dibromoacenaphthene

: 1642809-30-0
1,1-bis(4-fluorophenyl)-3,3-bis(4-methoxyphenyl)-1,2,5,7-tetrahydro-6-oxacyclopenta[cd]phenalene

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium / tetrahydrofuran; hexane / Flow reactor

2: n-butyllithium / tetrahydrofuran; hexane / Flow reactor

3: trifluoroacetic acid / dichloromethane / 17 h / 23 °C

With n-butyllithium; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1246/cl.130872