(2,3-dimethyl-1-oxo-1,3-diphenyl-2,3,3a,6-tetrahydro-1H-1λ⁵-benzo[c][1,2]azaphosphol-6-yl)-furan-2-yl-methanol

Base Information

• Chemical Name: (2,3-dimethyl-1-oxo-1,3-diphenyl-2,3,3a,6-tetrahydro-1H-1λ⁵-benzo[c][1,2]azaphosphol-6-yl)-furan-2-yl-methanol
• CAS No.: 874280-77-0
• Molecular Formula: C₂₆H₂₆NO₃P
• Molecular Weight: 431.471

Synonyms:(2,3-dimethyl-1-oxo-1,3-diphenyl-2,3,3a,6-tetrahydro-1H-1λ⁵-benzo[c][1,2]azaphosphol-6-yl)-furan-2-yl-methanol

Chemical Property of (2,3-dimethyl-1-oxo-1,3-diphenyl-2,3,3a,6-tetrahydro-1H-1λ⁵-benzo[c][1,2]azaphosphol-6-yl)-furan-2-yl-methanol

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Technology Process of (2,3-dimethyl-1-oxo-1,3-diphenyl-2,3,3a,6-tetrahydro-1H-1λ⁵-benzo[c][1,2]azaphosphol-6-yl)-furan-2-yl-methanol

There total 1 articles about (2,3-dimethyl-1-oxo-1,3-diphenyl-2,3,3a,6-tetrahydro-1H-1λ⁵-benzo[c][1,2]azaphosphol-6-yl)-furan-2-yl-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

furfural (98-01-1) + diphenylphosphinic acid N-methyl-(S)-α-methylbenzylamide (874280-81-6) → (2,3-dimethyl-1-oxo-1,3-diphenyl-2,3,3a,6-tetrahydro-1H-1λ5-benzo[c][1,2]azaphosphol-6-yl)-furan-2-yl-methanol (874280-77-0) + (2,3-dimethyl-1-oxo-1,3-diphenyl-2,3,3a,6-tetrahydro-1H-1λ5-benzo[c][1,2]azaphosphol-6-yl)-furan-2-yl-methanol

Guidance literature:

diphenylphosphinic acid N-methyl-(S)-α-methylbenzylamide; With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium; In tetrahydrofuran; cyclohexane; at -90 ℃; for 0.0166667h;

furfural; In tetrahydrofuran; cyclohexane; at -90 ℃; for 0.0166667h;

DOI:10.1039/b510685k

Reference yield: 95.0%

(2,3-dimethyl-1-oxo-1,3-diphenyl-2,3,3a,6-tetrahydro-1H-1λ5-benzo[c][1,2]azaphosphol-6-yl)-furan-2-yl-methanol (874280-77-0) → [3-(furan-2-yl-hydroxy-methyl)-6-(1-methylamino-1-phenyl-ethyl)-cyclohexa-1,4-dienyl]-phenyl-phosphinic acid

Guidance literature:

With hydrogenchloride; In acetone; at 20 ℃; for 0.5h;

DOI:10.1039/b510685k

upstream raw materials:

furfural

diphenylphosphinic acid N-methyl-(S)-α-methylbenzylamide

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