(R)-5-<(benzyloxy)methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

Base Information

Chemical Name:(R)-5-<(benzyloxy)methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone
CAS No.:173256-43-4
Molecular Formula:C₂₇H₄₂O₅
Molecular Weight:446.627
Hs Code.:

Synonyms:(R)-5-<(benzyloxy)methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

Suppliers and Price of (R)-5-<(benzyloxy)methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-5-<(benzyloxy)methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

Chemical Property:

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Technology Process of (R)-5-<(benzyloxy)methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

There total 9 articles about (R)-5-<(benzyloxy)methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 112-64-1
tetradecanoyl chloride

: 173256-42-3
(S)-5-<(benzyloxy)methyl>-5-(hydroxymethyl)tetrahydro-2-furanone

: 173256-43-4
(R)-5-<(benzyloxy)methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

Guidance literature:: With pyridine; dmap; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/jm950277n

Reference yield:

: 100-39-0
benzyl bromide

: 173256-43-4
(R)-5-<(benzyloxy)methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / Ag₂O / dimethylformamide / 120 h / Ambient temperature

2: 96 percent / aq. NaIO₄, OsO₄, 4-methylmorpholine N-oxide / acetone; 2-methyl-propan-2-ol / 20 h / Ambient temperature

3: 70 percent / NaBH₄ / methanol / 0.5 h / -10 °C

4: 92 percent / pyridine, (dimethylamino)pyridine / CH₂Cl₂ / 2 h / Ambient temperature

With pyridine; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide; silver(l) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide; acetone; tert-butyl alcohol;
DOI:10.1021/jm950277n

Reference yield:

: 173256-41-2
(S)-5-vinyl-5-(hydroxymethyl)tetrahydro-2-furanone

: 173256-43-4
(R)-5-<(benzyloxy)methyl>-5-<(tetradecanoyloxy)methyl>tetrahydro-2-furanone

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / Ag₂O / dimethylformamide / 120 h / Ambient temperature

2: 96 percent / aq. NaIO₄, OsO₄, 4-methylmorpholine N-oxide / acetone; 2-methyl-propan-2-ol / 20 h / Ambient temperature

3: 70 percent / NaBH₄ / methanol / 0.5 h / -10 °C

4: 92 percent / pyridine, (dimethylamino)pyridine / CH₂Cl₂ / 2 h / Ambient temperature

With pyridine; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide; silver(l) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide; acetone; tert-butyl alcohol;
DOI:10.1021/jm950277n