C₁₈H₂₆N₂O₅

Base Information

Chemical Name:C₁₈H₂₆N₂O₅
CAS No.:888970-67-0
Molecular Formula:C₁₈H₂₆N₂O₅
Molecular Weight:350.415
Hs Code.:

C<sub>18</sub>H<sub>26</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₁₈H₂₆N₂O₅

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Chemical Property of C₁₈H₂₆N₂O₅

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Technology Process of C₁₈H₂₆N₂O₅

There total 5 articles about C₁₈H₂₆N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1048654-48-3
C₁₅H₂₁NO₄

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 888970-67-0
C₁₈H₂₆N₂O₅

Guidance literature:: C₁₅H₂₁NO₄; glycine ethyl ester hydrochloride; With HATU; In dichloromethane; at 0 ℃; for 0.333333h; Inert atmosphere;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2011.06.032

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 888970-67-0
C₁₈H₂₆N₂O₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / water / 2 h

1.2: 60 h / 20 °C / Reflux

2.1: HATU / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

2.2: 24 h / 20 °C / Inert atmosphere

With potassium carbonate; HATU; In dichloromethane; water;
DOI:10.1016/j.tet.2011.06.032

Reference yield:

: 122-00-9
para-methylacetophenone

: 888970-67-0
C₁₈H₂₆N₂O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonium hydroxide / ethanol / 4 h / 60 - 65 °C

1.3: Auto-seeded programmed polythermic preferential crystallization; Resolution of racemate

2.1: sodium hydroxide / water / 72 h / Reflux

3.1: potassium carbonate / water / 2 h

3.2: 60 h / 20 °C / Reflux

4.1: HATU / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

4.2: 24 h / 20 °C / Inert atmosphere

With ammonium hydroxide; potassium carbonate; HATU; sodium hydroxide; In ethanol; dichloromethane; water; 1.1: Bucherer-Bergs reaction;
DOI:10.1016/j.tet.2011.06.032