methyl cis-5,6,6a,11a-tetrahydro-6-methyl-12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

Base Information

Chemical Name:methyl cis-5,6,6a,11a-tetrahydro-6-methyl-12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate
CAS No.:88939-79-1
Molecular Formula:C₂₈H₂₆N₂O₅S
Molecular Weight:502.591
Hs Code.:

Synonyms:methyl cis-5,6,6a,11a-tetrahydro-6-methyl-12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

Suppliers and Price of methyl cis-5,6,6a,11a-tetrahydro-6-methyl-12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl cis-5,6,6a,11a-tetrahydro-6-methyl-12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl cis-5,6,6a,11a-tetrahydro-6-methyl-12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

There total 6 articles about methyl cis-5,6,6a,11a-tetrahydro-6-methyl-12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 88939-72-4
[1-[3-Ethyl-1-(4-methoxy-benzenesulfonyl)-1H-indol-2-yl]-meth-(E)-ylidene]-(2-vinyl-phenyl)-amine

: 79-22-1
methyl chloroformate

: 88939-79-1
methyl cis-5,6,6a,11a-tetrahydro-6-methyl-12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

Guidance literature:: In chlorobenzene; for 6h; Heating;
DOI:10.1016/S0040-4020(01)88612-9

Reference yield:

: 88939-69-9
1-<(p-methoxyphenyl)sulfonyl>-3-ethylindole

: 88939-79-1
methyl cis-5,6,6a,11a-tetrahydro-6-methyl-12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / TiCl₄ / CH₂Cl₂ / 0.67 h / -35 °C

2: CH₂Cl₂

3: 81 percent / chlorobenzene / 6 h / Heating

With titanium tetrachloride; In dichloromethane; chlorobenzene;
DOI:10.1016/S0040-4020(01)88612-9

Reference yield:

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 88939-79-1
methyl cis-5,6,6a,11a-tetrahydro-6-methyl-12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH/mineral oil / 1.) THF, 5 deg C, 15 min; 20 deg C, 15 min; reflux 1 h; 2.) THF, 20 deg C, 1 h

2: 81 percent / TiCl₄ / CH₂Cl₂ / 0.67 h / -35 °C

3: CH₂Cl₂

4: 81 percent / chlorobenzene / 6 h / Heating

With titanium tetrachloride; sodium hydride; mineral oil; In dichloromethane; chlorobenzene;
DOI:10.1016/S0040-4020(01)88612-9