(4S,5R)-6-(tert-butyl-dimethylsilanyloxy)-4-methoxy-5-[(4-methoxybenzyl)oxy]hexanal

Base Information

Chemical Name:(4S,5R)-6-(tert-butyl-dimethylsilanyloxy)-4-methoxy-5-[(4-methoxybenzyl)oxy]hexanal
CAS No.:942505-85-3
Molecular Formula:C₂₁H₃₆O₅Si
Molecular Weight:396.599
Hs Code.:

Synonyms:(4S,5R)-6-(tert-butyl-dimethylsilanyloxy)-4-methoxy-5-[(4-methoxybenzyl)oxy]hexanal

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Chemical Property of (4S,5R)-6-(tert-butyl-dimethylsilanyloxy)-4-methoxy-5-[(4-methoxybenzyl)oxy]hexanal

Chemical Property:

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Technology Process of (4S,5R)-6-(tert-butyl-dimethylsilanyloxy)-4-methoxy-5-[(4-methoxybenzyl)oxy]hexanal

There total 7 articles about (4S,5R)-6-(tert-butyl-dimethylsilanyloxy)-4-methoxy-5-[(4-methoxybenzyl)oxy]hexanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₃₈O₅Si

: 942505-85-3
(4S,5R)-6-(tert-butyl-dimethylsilanyloxy)-4-methoxy-5-[(4-methoxybenzyl)oxy]hexanal

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane;
DOI:10.1039/b700827a

Reference yield:

: 952609-40-4
(2R,3S)-3-methoxy-hex-5-ene-1,2-diol

: 942505-85-3
(4S,5R)-6-(tert-butyl-dimethylsilanyloxy)-4-methoxy-5-[(4-methoxybenzyl)oxy]hexanal

Guidance literature:: Multi-step reaction with 4 steps

1.1: imidazole / CH₂Cl₂

2.1: TfOH / CH₂Cl₂

3.1: 9-BBN / tetrahydrofuran

3.2: H₂O₂ / pH 7

4.1: Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂

With 1H-imidazole; 9-borabicyclo[3.3.1]nonane dimer; trifluorormethanesulfonic acid; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b700827a

Reference yield:

: 942505-94-4
(S)-1-[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]-but-3-enyl methyl ether

: 942505-85-3
(4S,5R)-6-(tert-butyl-dimethylsilanyloxy)-4-methoxy-5-[(4-methoxybenzyl)oxy]hexanal

Guidance literature:: Multi-step reaction with 5 steps

1.1: p-TsOH / methanol

2.1: imidazole / CH₂Cl₂

3.1: TfOH / CH₂Cl₂

4.1: 9-BBN / tetrahydrofuran

4.2: H₂O₂ / pH 7

5.1: Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂

With 1H-imidazole; 9-borabicyclo[3.3.1]nonane dimer; trifluorormethanesulfonic acid; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/b700827a