(3S,4S)-6-(tert-Butyl-diphenyl-silanyloxy)-4-methoxymethoxy-3-methyl-hexanal

Base Information

Chemical Name:(3S,4S)-6-(tert-Butyl-diphenyl-silanyloxy)-4-methoxymethoxy-3-methyl-hexanal
CAS No.:899798-65-3
Molecular Formula:C₂₅H₃₆O₄Si
Molecular Weight:428.644
Hs Code.:

Synonyms:(3S,4S)-6-(tert-Butyl-diphenyl-silanyloxy)-4-methoxymethoxy-3-methyl-hexanal

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Chemical Property of (3S,4S)-6-(tert-Butyl-diphenyl-silanyloxy)-4-methoxymethoxy-3-methyl-hexanal

Chemical Property:

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Technology Process of (3S,4S)-6-(tert-Butyl-diphenyl-silanyloxy)-4-methoxymethoxy-3-methyl-hexanal

There total 4 articles about (3S,4S)-6-(tert-Butyl-diphenyl-silanyloxy)-4-methoxymethoxy-3-methyl-hexanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 899798-71-1
(3S,4S)-6-(tert-Butyl-diphenyl-silanyloxy)-4-methoxymethoxy-3-methyl-hexanenitrile

: 899798-65-3
(3S,4S)-6-(tert-Butyl-diphenyl-silanyloxy)-4-methoxymethoxy-3-methyl-hexanal

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1021/ol060669w

Reference yield:

: 899798-69-7
(2S,3S)-5-(tert-Butyl-diphenyl-silanyloxy)-3-methoxymethoxy-2-methyl-pentan-1-ol

: 899798-65-3
(3S,4S)-6-(tert-Butyl-diphenyl-silanyloxy)-4-methoxymethoxy-3-methyl-hexanal

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / Et₃N / CH₂Cl₂ / 16 h / 20 °C

2: 97 percent / dimethylsulfoxide / 2 h / 80 °C

3: diisobutylaluminum hydride / tetrahydrofuran; hexane / 3 h / 20 °C

With diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide;
DOI:10.1002/chem.200700342

Reference yield:

: 899798-67-5
(2R,3S)-5-(tert-Butyl-diphenyl-silanyloxy)-1-((1S,5R,7R)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-hydroxy-2-methyl-pentan-1-one

: 899798-65-3
(3S,4S)-6-(tert-Butyl-diphenyl-silanyloxy)-4-methoxymethoxy-3-methyl-hexanal

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / iPr₂NEt / CH₂Cl₂ / 4 h / Heating

2: 94 percent / LiAlH₄ / diethyl ether / 2 h / 0 °C

3: 87 percent / Et₃N / CH₂Cl₂ / 16 h / 20 °C

4: 97 percent / dimethylsulfoxide / 2 h / 80 °C

5: diisobutylaluminum hydride / tetrahydrofuran; hexane / 3 h / 20 °C

With lithium aluminium tetrahydride; diisobutylaluminium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide;
DOI:10.1002/chem.200700342