methyl (2R)-2-((R)-2-(tert-butoxycarbonylamino)propanamido)-3-phenylpropanoate

Base Information

Chemical Name:methyl (2R)-2-((R)-2-(tert-butoxycarbonylamino)propanamido)-3-phenylpropanoate
CAS No.:1093111-80-8
Molecular Formula:C₁₈H₂₆N₂O₅
Molecular Weight:350.415
Hs Code.:

Synonyms:methyl (2R)-2-((R)-2-(tert-butoxycarbonylamino)propanamido)-3-phenylpropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2R)-2-((R)-2-(tert-butoxycarbonylamino)propanamido)-3-phenylpropanoate

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Technology Process of methyl (2R)-2-((R)-2-(tert-butoxycarbonylamino)propanamido)-3-phenylpropanoate

There total 1 articles about methyl (2R)-2-((R)-2-(tert-butoxycarbonylamino)propanamido)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 3744-87-4,7764-95-6,15761-38-3
Boc-(R)-Ala

: 13033-84-6
D-phenylalanine methyl ester hydrochloride

: 1093111-80-8
methyl (2R)-2-((R)-2-(tert-butoxycarbonylamino)propanamido)-3-phenylpropanoate

Guidance literature:: Boc-(R)-Ala; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;

D-phenylalanine methyl ester hydrochloride; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo8020264

Reference yield:

: 1093111-80-8
methyl (2R)-2-((R)-2-(tert-butoxycarbonylamino)propanamido)-3-phenylpropanoate

: 313503-79-6
D-Ala-D-Phe-OMe

Guidance literature:: methyl (2R)-2-((R)-2-(tert-butoxycarbonylamino)propanamido)-3-phenylpropanoate; With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jo8020264