4-(benzotriazol-1-yl)-5-[4-(1-methyl-1-phenylethyl)phenoxy]phthalodinitrile

Base Information

Chemical Name:4-(benzotriazol-1-yl)-5-[4-(1-methyl-1-phenylethyl)phenoxy]phthalodinitrile
CAS No.:697239-05-7
Molecular Formula:C₂₉H₂₁N₅O
Molecular Weight:455.519
Hs Code.:

Synonyms:4-(benzotriazol-1-yl)-5-[4-(1-methyl-1-phenylethyl)phenoxy]phthalodinitrile

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Chemical Property of 4-(benzotriazol-1-yl)-5-[4-(1-methyl-1-phenylethyl)phenoxy]phthalodinitrile

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Technology Process of 4-(benzotriazol-1-yl)-5-[4-(1-methyl-1-phenylethyl)phenoxy]phthalodinitrile

There total 1 articles about 4-(benzotriazol-1-yl)-5-[4-(1-methyl-1-phenylethyl)phenoxy]phthalodinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 599-64-4
p-cumylphenol

: 274924-71-9
4-(1H-1,2,3-benzotriazol-1-yl)-5-nitrophthalonitrile

: 697239-05-7
4-(benzotriazol-1-yl)-5-[4-(1-methyl-1-phenylethyl)phenoxy]phthalodinitrile

Guidance literature:: With potassium carbonate; In water; N,N-dimethyl-formamide; at 20 ℃; for 0.5h;
DOI:10.1134/S1070363207090216

Reference yield: 76.8%

: 697239-05-7
4-(benzotriazol-1-yl)-5-[4-(1-methyl-1-phenylethyl)phenoxy]phthalodinitrile

: cobalt 3,10,17,24-tetra[4-(benzotriazol-1-yl)]-2,9,16,23-tetra{5-[4-(1-methyl-1-phenylethyl)phenoxy]}phthalocyanine

Guidance literature:: With cobalt(II) chloride; Heating;
DOI:10.1134/S1070363207090216

Reference yield: 76.8%

: 697239-05-7
4-(benzotriazol-1-yl)-5-[4-(1-methyl-1-phenylethyl)phenoxy]phthalodinitrile

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: cobalt tetra[4-(benzotriazol-1-yl)]-tetra(5-[4-(1-methyl-1-phenylethyl)phenoxy])phthalocyanine

Guidance literature:: In not given; mixt. was heated at 200-220°C for 1-1.5 h; solid was ground, washed with 5% HCl, washed with water to neutral, dried at 80°C, then extd. with CHCl3, solvent was removed, residue was treated with aq. acetone (1:10 v/v), chromd. on Al2O3 with CHCl3 as eluent; elem. anal.;
DOI:10.1134/S1070363207090216