4'-[2''-deoxy-5''-O-(4,4'-dimethoxytriphenylmethyl)-β-D-ribofuranosyl]-3,5-dinitrobiphenyl

Base Information

Chemical Name:4'-[2''-deoxy-5''-O-(4,4'-dimethoxytriphenylmethyl)-β-D-ribofuranosyl]-3,5-dinitrobiphenyl
CAS No.:912818-48-5
Molecular Formula:C₃₈H₃₄N₂O₉
Molecular Weight:662.696
Hs Code.:

Synonyms:4'-[2''-deoxy-5''-O-(4,4'-dimethoxytriphenylmethyl)-β-D-ribofuranosyl]-3,5-dinitrobiphenyl

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Chemical Property of 4'-[2''-deoxy-5''-O-(4,4'-dimethoxytriphenylmethyl)-β-D-ribofuranosyl]-3,5-dinitrobiphenyl

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Technology Process of 4'-[2''-deoxy-5''-O-(4,4'-dimethoxytriphenylmethyl)-β-D-ribofuranosyl]-3,5-dinitrobiphenyl

There total 10 articles about 4'-[2''-deoxy-5''-O-(4,4'-dimethoxytriphenylmethyl)-β-D-ribofuranosyl]-3,5-dinitrobiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 912818-42-9
4'-(2''-deoxy-β-D-ribofuranosyl)-3,5-dinitrobiphenyl

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 912818-48-5
4'-[2''-deoxy-5''-O-(4,4'-dimethoxytriphenylmethyl)-β-D-ribofuranosyl]-3,5-dinitrobiphenyl

Guidance literature:: With pyridine; at 20 ℃; for 4h;
DOI:10.1016/j.bmc.2006.05.072

Reference yield:

: 898828-50-7
4-(2'-deoxy-β-D-ribofuranosyl)-1-bromobenzene

: 912818-48-5
4'-[2''-deoxy-5''-O-(4,4'-dimethoxytriphenylmethyl)-β-D-ribofuranosyl]-3,5-dinitrobiphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: K₃PO₄ / Pd(PPh₃)4 / dimethylformamide / 16 h / 85 °C

2: 95 percent / pyridine / 4 h / 20 °C

With pyridine; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; 1: Suzuki coupling;
DOI:10.1016/j.bmc.2006.05.072

Reference yield:

: 428820-95-5
2-(3,5-dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 912818-48-5
4'-[2''-deoxy-5''-O-(4,4'-dimethoxytriphenylmethyl)-β-D-ribofuranosyl]-3,5-dinitrobiphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: K₃PO₄ / Pd(PPh₃)4 / dimethylformamide / 16 h / 85 °C

2: 95 percent / pyridine / 4 h / 20 °C

With pyridine; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; 1: Suzuki coupling;
DOI:10.1016/j.bmc.2006.05.072