2-(3,5-dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(3,5-dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:428820-95-5
Molecular Formula:C₁₂H₁₅BN₂O₆
Molecular Weight:294.072
Hs Code.:2931900090
Mol file:428820-95-5.mol

Synonyms:2-(3,5-dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Suppliers and Price of 2-(3,5-dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3,5-Dinitrophenylboronicacid,pinacolester
250mg
$ 175.00

TCI Chemical
2-(3,5-Dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane >98.0%(GC)
1g
$ 239.00

TCI Chemical
2-(3,5-Dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane >98.0%(GC)
200mg
$ 110.00

Chem-Impex
2-(3,5-Dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane,≥98%(GC) ≥98%(GC)
1G
$ 273.73

Chem-Impex
2-(3,5-Dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane,98%(GC) 98%(GC)
200MG
$ 101.92

AK Scientific
3,5-Dinitrophenylboronicacidpinacolester
250mg
$ 197.00

Total 13 raw suppliers

Chemical Property of 2-(3,5-dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property:

Melting Point:147.0 to 151.0 °C

Purity/Quality:

97% ^*data from raw suppliers

3,5-Dinitrophenylboronicacid,pinacolester ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(3,5-dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 4 articles about 2-(3,5-dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 6276-04-6
3,5-dinitroiodobenzene

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 428820-95-5
2-(3,5-dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine; In 1,4-dioxane; at 85 ℃; for 16h;
DOI:10.1016/j.bmc.2006.05.072

Reference yield: 40.0%

: 6276-04-6
3,5-dinitroiodobenzene

: 73183-34-3
bis(pinacol)diborane

: 428820-95-5
2-(3,5-dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In dimethyl sulfoxide; at 70 ℃; for 17h;

Reference yield:

: 618-87-1
3, 5-dinitroaniline

: 428820-95-5
2-(3,5-dinitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / water / 0.17 h / Inert atmosphere; Schlenk technique

1.2: 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

1.3: 1 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2.1: acetonitrile / Inert atmosphere; Schlenk technique

With hydrogenchloride; In water; acetonitrile;
DOI:10.1021/jacs.7b07444