n-propyldiphenyltin hydride

Base Information

Chemical Name:n-propyldiphenyltin hydride
CAS No.:153465-10-2
Molecular Formula:C₁₅H₁₈Sn
Molecular Weight:317.018
Hs Code.:

Synonyms:n-propyldiphenyltin hydride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of n-propyldiphenyltin hydride

Chemical Property:

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Technology Process of n-propyldiphenyltin hydride

There total 2 articles about n-propyldiphenyltin hydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1011-95-6
diphenyltin

: 106-94-5
propyl bromide

: 153465-10-2
n-propyldiphenyltin hydride

Guidance literature:: With n-butyllithium; water; diisopropylamine; In tetrahydrofuran; hexane; Petroleum ether; N2-atmosphere; stirring (0°C, 15 min), Sn-compd. addn. (-70°C), stirring (-50°C, 30 min), n-PrBr addn., petroleum ether addn. (0°C), H2O addn.; extg. (petroleum ether), washing (H2O), drying (MgSO4), evapn., distg.; elem. anal.;
DOI:10.1021/om960444x

Reference yield:

: 16853-85-3
lithium aluminium tetrahydride

: C₁₅H₁₇ClSn

: 153465-10-2
n-propyldiphenyltin hydride

Guidance literature:: In diethyl ether;
DOI:10.1139/cjc-2013-0504

Reference yield: 91.3%

: 153465-10-2
n-propyldiphenyltin hydride

: 1609183-87-0
(E)-N-(3-chloropropyl)-2,2-dimethylpropan-1-imine

: (E)-N-(3-(diphenyl(propyl)stannyl)propyl)-2,2-dimethylpropan-1-imine

Guidance literature:: n-propyldiphenyltin hydride; With lithium diisopropyl amide; In tetrahydrofuran; at 0 ℃; for 0.0833333h; Schlenk technique;

(E)-N-(3-chloropropyl)-2,2-dimethylpropan-1-imine; In tetrahydrofuran; at 0 - 20 ℃; for 0.166667h; Schlenk technique;
DOI:10.1139/cjc-2013-0504