C₂₆H₃₀O₈

Base Information

Chemical Name:C₂₆H₃₀O₈
CAS No.:306726-22-7
Molecular Formula:C₂₆H₃₀O₈
Molecular Weight:470.519
Hs Code.:

C<sub>26</sub>H<sub>30</sub>O<sub>8</sub>

Synonyms:C₂₆H₃₀O₈

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Chemical Property of C₂₆H₃₀O₈

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Technology Process of C₂₆H₃₀O₈

There total 15 articles about C₂₆H₃₀O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 306726-21-6
C₂₇H₃₄O₁₁S

: 306726-22-7
C₂₆H₃₀O₈

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; for 24h; Heating;
DOI:10.1002/1521-3765(20000901)6:17<3116::AID-CHEM3116>3.0.CO;2-8

Reference yield: 75.0%

: C₃₂H₃₈O₁₀Se

: 306726-22-7
C₂₆H₃₀O₈

Guidance literature:: With vinyl acetate; diisopropylamine; In toluene; at 140 ℃; for 12h;
DOI:10.1002/1521-3765(20000901)6:17<3166::AID-CHEM3166>3.0.CO;2-Z

Reference yield:

: 256341-98-7
(3aR,4S,7R,7aS)-2,2-Dimethyl-4-phenylselanyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ol

: 306726-22-7
C₂₆H₃₀O₈

Guidance literature:: Multi-step reaction with 11 steps

1.1: NaH / dimethylformamide / 0.08 h / 0 °C

1.2: 95 percent / nBu₄NI / dimethylformamide / 2 h / 0 - 25 °C

2.1: 96 percent / PPTS; MeOH / 1 h / 25 °C

3.1: 91 percent / 2,6-lutidine / tetrahydrofuran / 0.5 h / -78 °C

4.1: 100 percent / DAST / CH₂Cl₂ / 0.5 h / 0 °C

5.1: 0.71 g / SnCl₂ / diethyl ether / 3 h / 0 - 25 °C

6.1: 99 percent / NaOH / methanol / 1 h / 25 °C

7.1: aq. NaIO₄ / NaHCO₃ / CH₂Cl₂; methanol / 2 h / 25 °C

8.1: 0.120 g / iPr₂NH; vinyl acetate / toluene / 16 h / 140 °C

9.1: 98 percent / TBAF / tetrahydrofuran / 1 h / 25 °C

10.1: 97 percent / Et₃N / CH₂Cl₂ / 2 h / 0 - 25 °C

11.1: 87 percent / DBU / toluene / 24 h / Heating

With 2,6-dimethylpyridine; methanol; sodium hydroxide; sodium periodate; vinyl acetate; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; diisopropylamine; 4,4'-diaminostilbene-2,2'-disulfonic acid; tin(ll) chloride; sodium hydrogencarbonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene; 1.1: Metallation / 1.2: Etherification / 2.1: Ring cleavage / 3.1: Etherification / 4.1: Rearrangement / 5.1: Glycosidation / 6.1: Debenzoylation / 7.1: Oxidation / 8.1: Cyclization / 9.1: Silyl ether cleavage / 10.1: Mesylation / 11.1: Elimination;
DOI:10.1002/1521-3765(20000901)6:17<3116::AID-CHEM3116>3.0.CO;2-8