C₃₉H₅₀O₇Si

Base Information

Chemical Name:C₃₉H₅₀O₇Si
CAS No.:1182098-75-4
Molecular Formula:C₃₉H₅₀O₇Si
Molecular Weight:658.907
Hs Code.:

C<sub>39</sub>H<sub>50</sub>O<sub>7</sub>Si

Synonyms:C₃₉H₅₀O₇Si

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Chemical Property of C₃₉H₅₀O₇Si

Chemical Property:

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Technology Process of C₃₉H₅₀O₇Si

There total 45 articles about C₃₉H₅₀O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₀H₆₆O₈Si

: 1182098-75-4
C₃₉H₅₀O₇Si

Guidance literature:: With hydrogenchloride; palladium 10% on activated carbon; hydrogen; In methanol; water; ethyl acetate; at 20 ℃; for 4h;
DOI:10.1021/ol202265g

Reference yield:

: 1333325-37-3
1-benzyl 3-methyl 2,6-bis(benzyloxy)-4-(2-methoxy-2-oxoethyl)isophthalate

: 1182098-75-4
C₃₉H₅₀O₇Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 24 h / 0 - 20 °C

2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 3 h / 20 °C

3.1: ethylmagnesium bromide / tetrahydrofuran / 2.75 h / 0 - 50 °C

3.2: 0.03 h / 20 °C

4.1: (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole / tetrahydrofuran; Nitroethane / 1.3 h / -78 °C

5.1: platinum(IV) oxide; hydrogen / ethyl acetate / 3 h / 20 °C

6.1: Amberlyst 15.(R). / dichloromethane / 13 h / 20 °C

7.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -78 °C / Inert atmosphere

7.2: 3 h / 20 °C / Inert atmosphere

8.1: boron trifluoride diethyl etherate / dichloromethane / 0.25 h / -78 - 0 °C / Inert atmosphere

8.2: 0.5 h / -78 °C / Inert atmosphere

9.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol; water; ethyl acetate / 4 h / 20 °C

With hydrogenchloride; dmap; platinum(IV) oxide; lithium hydroxide monohydrate; palladium 10% on activated carbon; boron trifluoride diethyl etherate; ethylmagnesium bromide; water; hydrogen; diisobutylaluminium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole; In tetrahydrofuran; methanol; Nitroethane; dichloromethane; water; ethyl acetate; toluene;
DOI:10.1021/ol202265g

Reference yield:

: 1333325-39-5
1-benzyl 3-methyl 2,6-bis(benzyloxy)-4-(2-(methoxy(methyl)amino)-2-oxoethyl)isophthalate

: 1182098-75-4
C₃₉H₅₀O₇Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: ethylmagnesium bromide / tetrahydrofuran / 2.75 h / 0 - 50 °C

1.2: 0.03 h / 20 °C

2.1: (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole / tetrahydrofuran; Nitroethane / 1.3 h / -78 °C

3.1: platinum(IV) oxide; hydrogen / ethyl acetate / 3 h / 20 °C

4.1: Amberlyst 15.(R). / dichloromethane / 13 h / 20 °C

5.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -78 °C / Inert atmosphere

5.2: 3 h / 20 °C / Inert atmosphere

6.1: boron trifluoride diethyl etherate / dichloromethane / 0.25 h / -78 - 0 °C / Inert atmosphere

6.2: 0.5 h / -78 °C / Inert atmosphere

7.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol; water; ethyl acetate / 4 h / 20 °C

With hydrogenchloride; platinum(IV) oxide; palladium 10% on activated carbon; boron trifluoride diethyl etherate; ethylmagnesium bromide; hydrogen; diisobutylaluminium hydride; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole; In tetrahydrofuran; methanol; Nitroethane; dichloromethane; water; ethyl acetate; toluene;
DOI:10.1021/ol202265g