1,1,1,3,3,3-Hexafluoro-2-{2-[2-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-benzenesulfinyl]-phenyl}-propan-2-olatetetrabutyl-ammonium;

Base Information

• Chemical Name: 1,1,1,3,3,3-Hexafluoro-2-{2-[2-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-benzenesulfinyl]-phenyl}-propan-2-olatetetrabutyl-ammonium
• CAS No.: 80662-99-3
• Molecular Formula: C₁₆H₃₆N*C₁₈H₉F₁₂O₃S
• Molecular Weight: 775.783
• Mol file: 80662-99-3.mol

Synonyms:1,1,1,3,3,3-Hexafluoro-2-{2-[2-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-benzenesulfinyl]-phenyl}-propan-2-olatetetrabutyl-ammonium;

Chemical Property of 1,1,1,3,3,3-Hexafluoro-2-{2-[2-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-benzenesulfinyl]-phenyl}-propan-2-olatetetrabutyl-ammonium;

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1,1,3,3,3-Hexafluoro-2-{2-[2-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-benzenesulfinyl]-phenyl}-propan-2-olatetetrabutyl-ammonium;

There total 2 articles about 1,1,1,3,3,3-Hexafluoro-2-{2-[2-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-benzenesulfinyl]-phenyl}-propan-2-olatetetrabutyl-ammonium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

tetra(n-butyl)ammonium hydroxide (2052-49-5) + potassium salt of bis<2-(1,1,1,3,3,3-hexafluoro-2-hydroxypropyl)phenyl>sulfoxide (80662-97-1) → 1,1,1,3,3,3-Hexafluoro-2-{2-[2-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-benzenesulfinyl]-phenyl}-propan-2-olatetetrabutyl-ammonium; (80662-99-3)

Guidance literature:

In water;

DOI:10.1021/ja00370a039

Reference yield:

3,3,3',3'-Tetrakis(trifluoromethyl)-1,1'-spiro<3H-2,1-benzixathiole> (70091-68-8) → 1,1,1,3,3,3-Hexafluoro-2-{2-[2-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-benzenesulfinyl]-phenyl}-propan-2-olatetetrabutyl-ammonium; (80662-99-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / KOH / ethanol; H₂O / 168 h / Heating

2: 73 percent / H₂O

With potassium hydroxide; In ethanol; water;

DOI:10.1021/ja00370a039

upstream raw materials:

tetra(n-butyl)ammonium hydroxide

potassium salt of bis<2-(1,1,1,3,3,3-hexafluoro-2-hydroxypropyl)phenyl>sulfoxide

3,3,3',3'-Tetrakis(trifluoromethyl)-1,1'-spiro<3H-2,1-benzixathiole>