methyl 1-pentyl-2-[2-(phenylamino)-1,3-benzothiazol-7-yl]-1H-benzimidazole-5-carboxylate

Base Information

Chemical Name:methyl 1-pentyl-2-[2-(phenylamino)-1,3-benzothiazol-7-yl]-1H-benzimidazole-5-carboxylate
CAS No.:1428668-47-6
Molecular Formula:C₂₇H₂₆N₄O₂S
Molecular Weight:470.595
Hs Code.:

Synonyms:methyl 1-pentyl-2-[2-(phenylamino)-1,3-benzothiazol-7-yl]-1H-benzimidazole-5-carboxylate

Suppliers and Price of methyl 1-pentyl-2-[2-(phenylamino)-1,3-benzothiazol-7-yl]-1H-benzimidazole-5-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 1-pentyl-2-[2-(phenylamino)-1,3-benzothiazol-7-yl]-1H-benzimidazole-5-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 1-pentyl-2-[2-(phenylamino)-1,3-benzothiazol-7-yl]-1H-benzimidazole-5-carboxylate

There total 5 articles about methyl 1-pentyl-2-[2-(phenylamino)-1,3-benzothiazol-7-yl]-1H-benzimidazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1428668-33-0
C₂₀H₂₂ClN₃O₂

: 103-72-0
phenyl isothiocyanate

: 1428668-47-6
methyl 1-pentyl-2-[2-(phenylamino)-1,3-benzothiazol-7-yl]-1H-benzimidazole-5-carboxylate

Guidance literature:: With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate; In acetonitrile; at 140 ℃; for 0.666667h; Microwave irradiation; Inert atmosphere;
DOI:10.1039/c3ob27177c

Reference yield:

: 3970-35-2
2-chloro-3-nitrobezoic acid

: 1428668-47-6
methyl 1-pentyl-2-[2-(phenylamino)-1,3-benzothiazol-7-yl]-1H-benzimidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C / Inert atmosphere

2: trifluoroacetic acid; magnesium sulfate / 1,2-dichloro-ethane / Reflux; Inert atmosphere

3: zinc; ammonium formate / methanol / 0.17 h / 20 °C / Inert atmosphere

4: copper(l) iodide; 1,10-Phenanthroline; caesium carbonate / acetonitrile / 0.67 h / 140 °C / Microwave irradiation; Inert atmosphere

With dmap; copper(l) iodide; 1,10-Phenanthroline; ammonium formate; magnesium sulfate; caesium carbonate; dicyclohexyl-carbodiimide; trifluoroacetic acid; zinc; In methanol; dichloromethane; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1039/c3ob27177c

Reference yield:

: 1428668-27-2
C₂₀H₂₀ClN₃O₄

: 1428668-47-6
methyl 1-pentyl-2-[2-(phenylamino)-1,3-benzothiazol-7-yl]-1H-benzimidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: zinc; ammonium formate / methanol / 0.17 h / 20 °C / Inert atmosphere

2: copper(l) iodide; 1,10-Phenanthroline; caesium carbonate / acetonitrile / 0.67 h / 140 °C / Microwave irradiation; Inert atmosphere

With copper(l) iodide; 1,10-Phenanthroline; ammonium formate; caesium carbonate; zinc; In methanol; acetonitrile;
DOI:10.1039/c3ob27177c