4-fluoro-N-(4-methyl-5-(2-(4-oxo-3-phenylthiazolidin-2-ylidene)hydrazinecarbonyl)thiazol-2-yl)benzamide

Base Information

Chemical Name:4-fluoro-N-(4-methyl-5-(2-(4-oxo-3-phenylthiazolidin-2-ylidene)hydrazinecarbonyl)thiazol-2-yl)benzamide
CAS No.:1418192-05-8
Molecular Formula:C₂₁H₁₆FN₅O₃S₂
Molecular Weight:469.52
Hs Code.:

Synonyms:4-fluoro-N-(4-methyl-5-(2-(4-oxo-3-phenylthiazolidin-2-ylidene)hydrazinecarbonyl)thiazol-2-yl)benzamide

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Chemical Property of 4-fluoro-N-(4-methyl-5-(2-(4-oxo-3-phenylthiazolidin-2-ylidene)hydrazinecarbonyl)thiazol-2-yl)benzamide

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Technology Process of 4-fluoro-N-(4-methyl-5-(2-(4-oxo-3-phenylthiazolidin-2-ylidene)hydrazinecarbonyl)thiazol-2-yl)benzamide

There total 4 articles about 4-fluoro-N-(4-methyl-5-(2-(4-oxo-3-phenylthiazolidin-2-ylidene)hydrazinecarbonyl)thiazol-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1418192-04-7
4-fluoro-N-(4-methyl-5-(2-(phenylcarbamothioyl)hydrazinecarbonyl)thiazol-2-yl)benzamide

: 79-11-8
chloroacetic acid

: 1418192-05-8
4-fluoro-N-(4-methyl-5-(2-(4-oxo-3-phenylthiazolidin-2-ylidene)hydrazinecarbonyl)thiazol-2-yl)benzamide

Guidance literature:: With sodium acetate; In tetrahydrofuran; for 0.0833333h; Microwave irradiation; Inert atmosphere; Green chemistry;
DOI:10.1016/j.jfluchem.2012.10.012

Reference yield:

: 7210-76-6
ethyl-2-amino-4-methylthiazole-5-carboxylate

: 1418192-05-8
4-fluoro-N-(4-methyl-5-(2-(4-oxo-3-phenylthiazolidin-2-ylidene)hydrazinecarbonyl)thiazol-2-yl)benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / 0.03 h / Microwave irradiation; Inert atmosphere; Green chemistry

2: hydrazine hydrate / N,N-dimethyl-formamide / 0.02 h / Microwave irradiation; Inert atmosphere; Green chemistry

3: acetic acid / 0.07 h / Microwave irradiation; Inert atmosphere; Green chemistry

4: sodium acetate / tetrahydrofuran / 0.08 h / Microwave irradiation; Inert atmosphere; Green chemistry

With sodium acetate; hydrazine hydrate; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.jfluchem.2012.10.012

Reference yield:

: 403-43-0
4-fluorobenzoyl chloride

: 1418192-05-8
4-fluoro-N-(4-methyl-5-(2-(4-oxo-3-phenylthiazolidin-2-ylidene)hydrazinecarbonyl)thiazol-2-yl)benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / 0.03 h / Microwave irradiation; Inert atmosphere; Green chemistry

2: hydrazine hydrate / N,N-dimethyl-formamide / 0.02 h / Microwave irradiation; Inert atmosphere; Green chemistry

3: acetic acid / 0.07 h / Microwave irradiation; Inert atmosphere; Green chemistry

4: sodium acetate / tetrahydrofuran / 0.08 h / Microwave irradiation; Inert atmosphere; Green chemistry

With sodium acetate; hydrazine hydrate; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.jfluchem.2012.10.012