O-benzyl hex-2-en-1-yl[(N-tritylamino)methyl]phosphinate

Base Information

Chemical Name:O-benzyl hex-2-en-1-yl[(N-tritylamino)methyl]phosphinate
CAS No.:874292-07-6
Molecular Formula:C₃₃H₃₆NO₂P
Molecular Weight:509.628
Hs Code.:

Synonyms:O-benzyl hex-2-en-1-yl[(N-tritylamino)methyl]phosphinate

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Chemical Property of O-benzyl hex-2-en-1-yl[(N-tritylamino)methyl]phosphinate

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Technology Process of O-benzyl hex-2-en-1-yl[(N-tritylamino)methyl]phosphinate

There total 3 articles about O-benzyl hex-2-en-1-yl[(N-tritylamino)methyl]phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 874292-00-9
hex-2-en-1-ylphosphinic acid benzyl ester

: 120060-75-5
N-(triphenylmethyl)methanimine

: 874292-07-6
O-benzyl hex-2-en-1-yl[(N-tritylamino)methyl]phosphinate

Guidance literature:: With boron trifluoride diethyl etherate; In toluene; at 20 ℃; for 72h;
DOI:10.1021/jm050922i

Reference yield:

: 874291-94-8
((E)-Hex-2-enyl)-phosphinic acid

: 874292-07-6
O-benzyl hex-2-en-1-yl[(N-tritylamino)methyl]phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / tetrahydrofuran / 20 °C

2: 74 percent / BF₃*Et₂O / toluene / 72 h / 20 °C

With dmap; boron trifluoride diethyl etherate; dicyclohexyl-carbodiimide; In tetrahydrofuran; toluene;
DOI:10.1021/jm050922i

Reference yield:

: 118653-96-6
1-iodo-hex-2-ene

: 874292-07-6
O-benzyl hex-2-en-1-yl[(N-tritylamino)methyl]phosphinate

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium phosphinate; hexamethyldisilazane / CH₂Cl₂ / 20 °C

2: dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / tetrahydrofuran / 20 °C

3: 74 percent / BF₃*Et₂O / toluene / 72 h / 20 °C

With dmap; ammonium hypophosphite; boron trifluoride diethyl etherate; dicyclohexyl-carbodiimide; 1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jm050922i