methyl 4-((6,7-difluoro-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

Base Information

Chemical Name:methyl 4-((6,7-difluoro-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate
CAS No.:1432509-30-2
Molecular Formula:C₂₃H₂₁F₂NO₃
Molecular Weight:397.421
Hs Code.:

Synonyms:methyl 4-((6,7-difluoro-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

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Chemical Property of methyl 4-((6,7-difluoro-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

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Technology Process of methyl 4-((6,7-difluoro-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

There total 3 articles about methyl 4-((6,7-difluoro-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 2417-72-3
Methyl 4-(bromomethyl)benzoate

: 1432509-29-9
6,7-difluoro-2,2-dimethyl-2,3-dihydro-1H-carbazol-4(9H)-one

: 1432509-30-2
methyl 4-((6,7-difluoro-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

Guidance literature:: 6,7-difluoro-2,2-dimethyl-2,3-dihydro-1H-carbazol-4(9H)-one; With sodium hydride; In N,N-dimethyl-formamide; paraffin oil; for 0.166667h;

Methyl 4-(bromomethyl)benzoate; In N,N-dimethyl-formamide; paraffin oil; at 20 ℃; for 5h;

Reference yield:

: 126-81-8
dimedone

: 1432509-30-2
methyl 4-((6,7-difluoro-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / 0.17 h / 140 °C / Microwave irradiation

2.1: sodium hydride / N,N-dimethyl-formamide; paraffin oil / 0.17 h

2.2: 5 h / 20 °C

With sodium hydride; trifluoroacetic acid; In N,N-dimethyl-formamide; paraffin oil; 1.1: |Fischer Indole Synthesis;

Reference yield:

: 40594-37-4,875664-54-3
(3,4-difluorophenyl)phenylhydrazine hydrochloride

: 1432509-30-2
methyl 4-((6,7-difluoro-2,2-dimethyl-4-oxo-1,2,3,4-tetrahydrocarbazol-9-yl)methyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / 0.17 h / 140 °C / Microwave irradiation

2.1: sodium hydride / N,N-dimethyl-formamide; paraffin oil / 0.17 h

2.2: 5 h / 20 °C

With sodium hydride; trifluoroacetic acid; In N,N-dimethyl-formamide; paraffin oil; 1.1: |Fischer Indole Synthesis;