N-benzyloxycarbonyl-O-(3,4,6-tri-O-acetyl-2-N-allyloxycarbonylamino-2-deoxy-β-D-glucopyranosyl)-seryl-alanine tert-butyl ester

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Chemical Name:N-benzyloxycarbonyl-O-(3,4,6-tri-O-acetyl-2-N-allyloxycarbonylamino-2-deoxy-β-D-glucopyranosyl)-seryl-alanine tert-butyl ester
CAS No.:144923-63-7
Molecular Formula:C₃₄H₄₇N₃O₁₅
Molecular Weight:737.758
Hs Code.:

Synonyms:N-benzyloxycarbonyl-O-(3,4,6-tri-O-acetyl-2-N-allyloxycarbonylamino-2-deoxy-β-D-glucopyranosyl)-seryl-alanine tert-butyl ester

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Chemical Property of N-benzyloxycarbonyl-O-(3,4,6-tri-O-acetyl-2-N-allyloxycarbonylamino-2-deoxy-β-D-glucopyranosyl)-seryl-alanine tert-butyl ester

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Technology Process of N-benzyloxycarbonyl-O-(3,4,6-tri-O-acetyl-2-N-allyloxycarbonylamino-2-deoxy-β-D-glucopyranosyl)-seryl-alanine tert-butyl ester

There total 2 articles about N-benzyloxycarbonyl-O-(3,4,6-tri-O-acetyl-2-N-allyloxycarbonylamino-2-deoxy-β-D-glucopyranosyl)-seryl-alanine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 24864-42-4
N-benzyloxycarbonyl-seryl-alanine tert-butyl ester

: 863997-29-9
ethyl 3,4,6-tri-O-acetyl-2-allyloxycarbonylamino-2-deoxy-1-thio-β-D-glucopyranoside

: 144923-63-7
N-benzyloxycarbonyl-O-(3,4,6-tri-O-acetyl-2-N-allyloxycarbonylamino-2-deoxy-β-D-glucopyranosyl)-seryl-alanine tert-butyl ester

Guidance literature:: With 4 A molecular sieve; mercury(II) cyanide; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4039(00)79082-4

Reference yield: 54.0%

: 104655-87-0
3,4,6-tri-O-acetyl-2-N-allyloxycarbonyl-2-amino-2-deoxy-α-D-glucopyranosyl bromide

: 24864-42-4
N-benzyloxycarbonyl-seryl-alanine tert-butyl ester

: 144923-63-7
N-benzyloxycarbonyl-O-(3,4,6-tri-O-acetyl-2-N-allyloxycarbonylamino-2-deoxy-β-D-glucopyranosyl)-seryl-alanine tert-butyl ester

Guidance literature:: With 4 A molecular sieve; mercury(II) cyanide; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1016/S0957-4166(00)80230-X

Reference yield: 75.0%

: 144923-63-7
N-benzyloxycarbonyl-O-(3,4,6-tri-O-acetyl-2-N-allyloxycarbonylamino-2-deoxy-β-D-glucopyranosyl)-seryl-alanine tert-butyl ester

: (S)-2-[(S)-2-Benzyloxycarbonylamino-3-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-amino-tetrahydro-pyran-2-yloxy)-propionylamino]-propionic acid tert-butyl ester

Guidance literature:: With malonic acid dimethyl ester; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)79082-4