N'-methoxy-4-(1-methyl-1-{4-methyl-5-[2-(trifluoromethyl)phenyl]-4H-1,2,4-triazol-3-yl}ethoxy)benzenecarboxyimidamide

Base Information

Chemical Name:N'-methoxy-4-(1-methyl-1-{4-methyl-5-[2-(trifluoromethyl)phenyl]-4H-1,2,4-triazol-3-yl}ethoxy)benzenecarboxyimidamide
CAS No.:1203938-63-9
Molecular Formula:C₂₁H₂₂F₃N₅O₂
Molecular Weight:433.433
Hs Code.:

Synonyms:N'-methoxy-4-(1-methyl-1-{4-methyl-5-[2-(trifluoromethyl)phenyl]-4H-1,2,4-triazol-3-yl}ethoxy)benzenecarboxyimidamide

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Chemical Property of N'-methoxy-4-(1-methyl-1-{4-methyl-5-[2-(trifluoromethyl)phenyl]-4H-1,2,4-triazol-3-yl}ethoxy)benzenecarboxyimidamide

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Technology Process of N'-methoxy-4-(1-methyl-1-{4-methyl-5-[2-(trifluoromethyl)phenyl]-4H-1,2,4-triazol-3-yl}ethoxy)benzenecarboxyimidamide

There total 4 articles about N'-methoxy-4-(1-methyl-1-{4-methyl-5-[2-(trifluoromethyl)phenyl]-4H-1,2,4-triazol-3-yl}ethoxy)benzenecarboxyimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1203938-53-7
N'-hydroxy-4-(1-methyl-1-{4-methyl-5-[2-(trifluoromethyl)phenyl]-4H-1,2,4-triazol-3-yl}ethoxy)benzenecarboxyimidamide

: 74-88-4
methyl iodide

: 1203938-63-9
N'-methoxy-4-(1-methyl-1-{4-methyl-5-[2-(trifluoromethyl)phenyl]-4H-1,2,4-triazol-3-yl}ethoxy)benzenecarboxyimidamide

Guidance literature:: N'-hydroxy-4-(1-methyl-1-{4-methyl-5-[2-(trifluoromethyl)phenyl]-4H-1,2,4-triazol-3-yl}ethoxy)benzenecarboxyimidamide; With sodium hydride; In N,N-dimethyl-formamide; for 0.166667h;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

: 171426-41-8
N-methyl-2-(trifluoromethyl)benzamide

: 1203938-63-9
N'-methoxy-4-(1-methyl-1-{4-methyl-5-[2-(trifluoromethyl)phenyl]-4H-1,2,4-triazol-3-yl}ethoxy)benzenecarboxyimidamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride / N,N-dimethyl-formamide / chloroform / 20 - 60 °C

2.1: N,N-dimethyl-formamide; toluene / 3 h / 60 °C

3.1: hydroxylamine / ethanol / 3 h / 80 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h

4.2: 2 h / 20 °C

With thionyl chloride; hydroxylamine; sodium hydride; N,N-dimethyl-formamide; In ethanol; chloroform; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1203938-51-5
4-(1-methyl-1-{4-methyl-5-[2-(trifluoromethyl)phenyl]-4H-1,2,4-triazol-3-yl}ethoxy]benzonitrile

: 1203938-63-9
N'-methoxy-4-(1-methyl-1-{4-methyl-5-[2-(trifluoromethyl)phenyl]-4H-1,2,4-triazol-3-yl}ethoxy)benzenecarboxyimidamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxylamine / ethanol / 3 h / 80 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h

2.2: 2 h / 20 °C

With hydroxylamine; sodium hydride; In ethanol; N,N-dimethyl-formamide;