2-(5,6-diethoxy-7-fluoro-1-imino-1,3-dihydroisoindol-2-yl)-1-[3-ethoxy-5-(pentafluorosulfanyl)phenyl]ethanone hydrobromide

Base Information

Chemical Name:2-(5,6-diethoxy-7-fluoro-1-imino-1,3-dihydroisoindol-2-yl)-1-[3-ethoxy-5-(pentafluorosulfanyl)phenyl]ethanone hydrobromide
CAS No.:1180486-51-4
Molecular Formula:BrH*C₂₂H₂₄F₆N₂O₄S
Molecular Weight:607.412
Hs Code.:

Synonyms:2-(5,6-diethoxy-7-fluoro-1-imino-1,3-dihydroisoindol-2-yl)-1-[3-ethoxy-5-(pentafluorosulfanyl)phenyl]ethanone hydrobromide

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Chemical Property of 2-(5,6-diethoxy-7-fluoro-1-imino-1,3-dihydroisoindol-2-yl)-1-[3-ethoxy-5-(pentafluorosulfanyl)phenyl]ethanone hydrobromide

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Technology Process of 2-(5,6-diethoxy-7-fluoro-1-imino-1,3-dihydroisoindol-2-yl)-1-[3-ethoxy-5-(pentafluorosulfanyl)phenyl]ethanone hydrobromide

There total 4 articles about 2-(5,6-diethoxy-7-fluoro-1-imino-1,3-dihydroisoindol-2-yl)-1-[3-ethoxy-5-(pentafluorosulfanyl)phenyl]ethanone hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 474554-46-6
5,6-diethoxy-7-fluoro-3H-isoindol-1-ylamine

: 1178584-40-1
2-bromo-1-[3-ethoxy-5-(pentafluorosulfanyl)phenyl]ethanone

: 1180486-51-4
2-(5,6-diethoxy-7-fluoro-1-imino-1,3-dihydroisoindol-2-yl)-1-[3-ethoxy-5-(pentafluorosulfanyl)phenyl]ethanone hydrobromide

Guidance literature:: In tetrahydrofuran; at 20 - 25 ℃; Inert atmosphere;

Reference yield:

: 1178585-15-3
3-ethoxy-N-methoxy-N-methyl-5-(pentafluorosulfanyl)benzamide

: 1180486-51-4
2-(5,6-diethoxy-7-fluoro-1-imino-1,3-dihydroisoindol-2-yl)-1-[3-ethoxy-5-(pentafluorosulfanyl)phenyl]ethanone hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether; tetrahydrofuran / 0 - 25 °C / Inert atmosphere

2: phenyltrimethylammonium tribromide / tetrahydrofuran / 3 h / 20 - 25 °C / Inert atmosphere

3: tetrahydrofuran / 20 - 25 °C / Inert atmosphere

With phenyltrimethylammonium tribromide; In tetrahydrofuran; diethyl ether;

Reference yield:

: 1178585-29-9
ethyl 3-ethoxy-5-(pentafluorosulfanyl)benzoate

: 1180486-51-4
2-(5,6-diethoxy-7-fluoro-1-imino-1,3-dihydroisoindol-2-yl)-1-[3-ethoxy-5-(pentafluorosulfanyl)phenyl]ethanone hydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1: isopropylmagnesium chloride / tetrahydrofuran / 1.5 h / -15 - 25 °C / Inert atmosphere

2: diethyl ether; tetrahydrofuran / 0 - 25 °C / Inert atmosphere

3: phenyltrimethylammonium tribromide / tetrahydrofuran / 3 h / 20 - 25 °C / Inert atmosphere

4: tetrahydrofuran / 20 - 25 °C / Inert atmosphere

With isopropylmagnesium chloride; phenyltrimethylammonium tribromide; In tetrahydrofuran; diethyl ether;