[ReF(CO)(NO)(P(C₆H₅)3)3]⁽¹⁺⁾*BF₄^(1-)=[ReF(CO)(NO)(P(C₆H₅)3)3]BF₄

Base Information

Chemical Name:[ReF(CO)(NO)(P(C₆H₅)3)3]⁽¹⁺⁾*BF₄^(1-)=[ReF(CO)(NO)(P(C₆H₅)3)3]BF₄
CAS No.:83095-53-8
Molecular Formula:BF₄*C₅₅H₄₅FNO₂P₃Re
Molecular Weight:1136.9
Hs Code.:

[ReF(CO)(NO)(P(C<sub>6</sub>H<sub>5</sub>)3)3]<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>=[ReF(CO)(NO)(P(C<sub>6</sub>H<sub>5</sub>)3)3]BF<sub>4</sub>

Synonyms:[ReF(CO)(NO)(P(C₆H₅)3)3]⁽¹⁺⁾*BF₄^(1-)=[ReF(CO)(NO)(P(C₆H₅)3)3]BF₄

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Chemical Property of [ReF(CO)(NO)(P(C₆H₅)3)3]⁽¹⁺⁾*BF₄^(1-)=[ReF(CO)(NO)(P(C₆H₅)3)3]BF₄

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Technology Process of [ReF(CO)(NO)(P(C₆H₅)3)3]⁽¹⁺⁾*BF₄^(1-)=[ReF(CO)(NO)(P(C₆H₅)3)3]BF₄

There total 1 articles about [ReF(CO)(NO)(P(C₆H₅)3)3]⁽¹⁺⁾*BF₄^(1-)=[ReF(CO)(NO)(P(C₆H₅)3)3]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tetrafluoroboric acid

: 58694-74-9
[ReH₂(NO)(P(C₆H₅)3)3]

: 83095-53-8
[ReF(CO)(NO)(P(C₆H₅)3)3]⁽¹⁺⁾*BF₄^(1-)=[ReF(CO)(NO)(P(C₆H₅)3)3]BF₄

Guidance literature:: With CO; In ethanol; dichloromethane; High Pressure; a soln. of complex was treated with HBF4 and subjected to CO pressure (40 psi) for 20 min; solvent was removed, ppt. was recrystd. from CH2Cl2-cyclohexane-EtOH;elem.anal.;

Reference yield: 83.0%

: 83095-53-8
[ReF(CO)(NO)(P(C₆H₅)3)3]⁽¹⁺⁾*BF₄^(1-)=[ReF(CO)(NO)(P(C₆H₅)3)3]BF₄

: 124-41-4
sodium methylate

: 83114-90-3
[ReF(OCH₃)(CO)(NO)(P(C₆H₅)3)2]

Guidance literature:: In methanol; reagents were mixed, soln. was stirred for 15 min; solvent was removed, ppt. was recrystd. from CH2Cl2-MeOH;elem.anal.;

Reference yield: 60.0%

: 83095-53-8
[ReF(CO)(NO)(P(C₆H₅)3)3]⁽¹⁺⁾*BF₄^(1-)=[ReF(CO)(NO)(P(C₆H₅)3)3]BF₄

: 83095-55-0
[ReF₂(CO)(NO)(P(C₆H₅)3)2]

Guidance literature:: With KF; In ethanol; dichloromethane; to a soln. of complex in CH2Cl2 was added KF in EtOH, the soln. was heated under reflux for 40 min; solvent was removed, ppt. was recrystd. from CH2Cl2-EtOH;elem.anal.;