1-methyl-3-(α,α,β,β-tetrafluoroethyl)imidazolium 2,4,6-tris(fluorosulfonyl)phenolate

Base Information

• Chemical Name: 1-methyl-3-(α,α,β,β-tetrafluoroethyl)imidazolium 2,4,6-tris(fluorosulfonyl)phenolate
• CAS No.: 1423009-78-2
• Molecular Formula: C₆H₂F₃O₇S₃*C₆H₇F₄N₂
• Molecular Weight: 522.399

Synonyms:1-methyl-3-(α,α,β,β-tetrafluoroethyl)imidazolium 2,4,6-tris(fluorosulfonyl)phenolate

Chemical Property of 1-methyl-3-(α,α,β,β-tetrafluoroethyl)imidazolium 2,4,6-tris(fluorosulfonyl)phenolate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 1-methyl-3-(α,α,β,β-tetrafluoroethyl)imidazolium 2,4,6-tris(fluorosulfonyl)phenolate

There total 2 articles about 1-methyl-3-(α,α,β,β-tetrafluoroethyl)imidazolium 2,4,6-tris(fluorosulfonyl)phenolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,4,6-tris(fluorosulfonyl)anisole (1409940-17-5) + N-(α,α,β,β-tetrafluoroethyl)imidazole (91047-49-3) → 1-methyl-3-(α,α,β,β-tetrafluoroethyl)imidazolium 2,4,6-tris(fluorosulfonyl)phenolate (1423009-78-2)

Guidance literature:

In benzene; at 20 ℃; for 1h;

DOI:10.1016/j.jfluchem.2012.05.015

Reference yield:

2,4,6-tris(fluorosulfonyl)chlorobenzene → 1-methyl-3-(α,α,β,β-tetrafluoroethyl)imidazolium 2,4,6-tris(fluorosulfonyl)phenolate (1423009-78-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: methanol / 1 h / Reflux

2.1: silver carbonate / water / 2 h / 60 °C

2.2: 16 h / 20 °C

3.1: benzene / 1 h / 20 °C

With methanol; silver carbonate; In water; benzene;

DOI:10.1016/j.jfluchem.2012.05.015

upstream raw materials:

2,4,6-tris(fluorosulfonyl)anisole

N-(α,α,β,β-tetrafluoroethyl)imidazole

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