4-[4-(4,5-dihydro-1,2,4-(4H)-5-oxo-oxadiazol-3-ylmethyl)]-N-2,2,2-trichloroethoxycarbonylaniline

Base Information

Chemical Name:4-[4-(4,5-dihydro-1,2,4-(4H)-5-oxo-oxadiazol-3-ylmethyl)]-N-2,2,2-trichloroethoxycarbonylaniline
CAS No.:1229613-13-1
Molecular Formula:C₁₂H₁₀Cl₃N₃O₄
Molecular Weight:366.588
Hs Code.:

Synonyms:4-[4-(4,5-dihydro-1,2,4-(4H)-5-oxo-oxadiazol-3-ylmethyl)]-N-2,2,2-trichloroethoxycarbonylaniline

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Chemical Property of 4-[4-(4,5-dihydro-1,2,4-(4H)-5-oxo-oxadiazol-3-ylmethyl)]-N-2,2,2-trichloroethoxycarbonylaniline

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Technology Process of 4-[4-(4,5-dihydro-1,2,4-(4H)-5-oxo-oxadiazol-3-ylmethyl)]-N-2,2,2-trichloroethoxycarbonylaniline

There total 1 articles about 4-[4-(4,5-dihydro-1,2,4-(4H)-5-oxo-oxadiazol-3-ylmethyl)]-N-2,2,2-trichloroethoxycarbonylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1229613-12-0
4-(N-hydroxyamidinomethyl)-N-2,2,2-trichloroethoxycarbonylaniline

: 1885-14-9
phenyl chloroformate

: 1229613-13-1
4-[4-(4,5-dihydro-1,2,4-(4H)-5-oxo-oxadiazol-3-ylmethyl)]-N-2,2,2-trichloroethoxycarbonylaniline

Guidance literature:: 4-(N-hydroxyamidinomethyl)-N-2,2,2-trichloroethoxycarbonylaniline; phenyl chloroformate; With triethylamine; In tetrahydrofuran; at 0 ℃; Cooling with ice;

In toluene; for 4h; Reflux;
DOI:10.1016/j.bmc.2010.03.049