2,2-Dimethyl-propionic acid (1S,3S)-2-oxo-3-phenethyl-cyclobutylmethyl ester

Base Information

Chemical Name:2,2-Dimethyl-propionic acid (1S,3S)-2-oxo-3-phenethyl-cyclobutylmethyl ester
CAS No.:84851-88-7
Molecular Formula:C₁₈H₂₄O₃
Molecular Weight:288.387
Hs Code.:

Synonyms:2,2-Dimethyl-propionic acid (1S,3S)-2-oxo-3-phenethyl-cyclobutylmethyl ester

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Chemical Property of 2,2-Dimethyl-propionic acid (1S,3S)-2-oxo-3-phenethyl-cyclobutylmethyl ester

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Technology Process of 2,2-Dimethyl-propionic acid (1S,3S)-2-oxo-3-phenethyl-cyclobutylmethyl ester

There total 3 articles about 2,2-Dimethyl-propionic acid (1S,3S)-2-oxo-3-phenethyl-cyclobutylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 84851-81-0,84894-14-4
2,2-Dimethyl-propionic acid 2-(1-hydroxy-3-phenyl-propyl)-2-phenylsulfanyl-cyclopropylmethyl ester

: 84851-88-7
2,2-Dimethyl-propionic acid (1S,3S)-2-oxo-3-phenethyl-cyclobutylmethyl ester

Guidance literature:: With trimethoxonium tetrafluoroborate; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/jo00155a050

Reference yield:

: 84851-74-1
1-(2-Hydroxymethyl-1-phenylsulfanyl-cyclopropyl)-3-phenyl-propan-1-ol

: 84851-88-7
2,2-Dimethyl-propionic acid (1S,3S)-2-oxo-3-phenethyl-cyclobutylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: DMAP, C₅H₅N / CH₂Cl₂ / 0 °C

2: 55 percent / trimethyloxonium fluoroborate / CH₂Cl₂ / 2 h / Ambient temperature

With pyridine; dmap; trimethoxonium tetrafluoroborate; In dichloromethane;
DOI:10.1021/jo00155a050

Reference yield:

: 80398-85-2
1-Phenylsulfanyl-3-oxa-bicyclo[3.1.0]hexan-2-ol

: 84851-88-7
2,2-Dimethyl-propionic acid (1S,3S)-2-oxo-3-phenethyl-cyclobutylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 0 °C

2: DMAP, C₅H₅N / CH₂Cl₂ / 0 °C

3: 55 percent / trimethyloxonium fluoroborate / CH₂Cl₂ / 2 h / Ambient temperature

With pyridine; dmap; trimethoxonium tetrafluoroborate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00155a050