(p-ClC₆H₄)2BiI

Base Information

• Chemical Name: (p-ClC₆H₄)2BiI
• CAS No.: 121900-07-0
• Molecular Formula: C₁₂H₈BiCl₂I
• Molecular Weight: 558.986
• Mol file: 121900-07-0.mol

Synonyms:(p-ClC₆H₄)2BiI

Chemical Property of (p-ClC₆H₄)2BiI

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (p-ClC₆H₄)2BiI

There total 11 articles about (p-ClC₆H₄)2BiI which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.7%

chlorobis(4-chlorophenyl)bismuthane (51752-31-9) + sodium iodide (7681-82-5,24359-64-6,41927-88-2,115813-40-6) → (p-ClC6H4)2BiI (121900-07-0)

Guidance literature:

In ethanol;

Reference yield:

tris(4-chlorophenyl)bismuthane (5575-51-9) → 1-Chloro-4-iodobenzene (637-87-6) + (p-ClC6H4)2BiI (121900-07-0)

Guidance literature:

With iodine; In chloroform; molar ratio Bi(C6H4-p-Cl)3:Br2 = 1:1;

DOI:10.1039/CT9222100104

Reference yield:

4,4'-dibromodiphenyliodonium chloride (53601-22-2) → 1-Chloro-4-iodobenzene (637-87-6) + (p-ClC6H4)2BiI (121900-07-0)

Guidance literature:

Multi-step reaction with 4 steps

1: acetone

2: Br₂ / chloroform

3: diethyl ether

4: I₂ / chloroform

With Br₂; I₂; In diethyl ether; chloroform; acetone;

upstream raw materials:

tris(4-chlorophenyl)bismuthane

chlorobis(4-chlorophenyl)bismuthane

sodium iodide

4,4'-dibromodiphenyliodonium chloride

Downstream raw materials:

(p-ClC₆H₄)2Bi(1-C₁₀H₇)

(2-acetylphenyl)bromo(4-chlorophenyl)bismuthane

Refernces