1-{[(4-phenyl-4H-1,2,4-triazol-3-yl)sulfanyl]acetyl}-4-phenylthiosemicarbazide

Base Information

Chemical Name:1-{[(4-phenyl-4H-1,2,4-triazol-3-yl)sulfanyl]acetyl}-4-phenylthiosemicarbazide
CAS No.:6264-24-0
Molecular Formula:C₁₇H₁₆N₆OS₂
Molecular Weight:384.486
Hs Code.:

Synonyms:1-{[(4-phenyl-4H-1,2,4-triazol-3-yl)sulfanyl]acetyl}-4-phenylthiosemicarbazide

Suppliers and Price of 1-{[(4-phenyl-4H-1,2,4-triazol-3-yl)sulfanyl]acetyl}-4-phenylthiosemicarbazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-{[(4-phenyl-4H-1,2,4-triazol-3-yl)sulfanyl]acetyl}-4-phenylthiosemicarbazide

Chemical Property:

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Technology Process of 1-{[(4-phenyl-4H-1,2,4-triazol-3-yl)sulfanyl]acetyl}-4-phenylthiosemicarbazide

There total 5 articles about 1-{[(4-phenyl-4H-1,2,4-triazol-3-yl)sulfanyl]acetyl}-4-phenylthiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.5%

: 103-72-0
phenyl isothiocyanate

: 59909-04-5
[(4-phenyl-4H-1,2,4-triazol-3-yl)sulfanyl]acetohydrazide

: 6264-24-0
1-{[(4-phenyl-4H-1,2,4-triazol-3-yl)sulfanyl]acetyl}-4-phenylthiosemicarbazide

Guidance literature:: at 50 ℃; for 12h;
DOI:10.1002/jhet.563

Reference yield:

: 1-formyl-4-phenyl-3-thiosemicarbazide

: 6264-24-0
1-{[(4-phenyl-4H-1,2,4-triazol-3-yl)sulfanyl]acetyl}-4-phenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 4 steps

1: Alkaline conditions

2: sodium ethanolate / ethanol / 17 h / 25 °C / Reflux

3: hydrazine hydrate / ethanol / 24 h / 25 °C

4: 12 h / 50 °C

With sodium ethanolate; hydrazine hydrate; In ethanol;
DOI:10.1002/jhet.563

Reference yield:

: 5373-72-8
4-phenyl-Δ²-1,2,4-triazoline-5-thione

: 6264-24-0
1-{[(4-phenyl-4H-1,2,4-triazol-3-yl)sulfanyl]acetyl}-4-phenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium ethanolate / ethanol / 17 h / 25 °C / Reflux

2: hydrazine hydrate / ethanol / 24 h / 25 °C

3: 12 h / 50 °C

With sodium ethanolate; hydrazine hydrate; In ethanol;
DOI:10.1002/jhet.563