(1R,2S,3S,6R)-2-hydroxy-6-methyl-3-(methylethyl)cyclohexyl methylsulfonate

Base Information

Chemical Name:(1R,2S,3S,6R)-2-hydroxy-6-methyl-3-(methylethyl)cyclohexyl methylsulfonate
CAS No.:308239-17-0
Molecular Formula:C₁₁H₂₂O₄S
Molecular Weight:250.359
Hs Code.:

Synonyms:(1R,2S,3S,6R)-2-hydroxy-6-methyl-3-(methylethyl)cyclohexyl methylsulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,3S,6R)-2-hydroxy-6-methyl-3-(methylethyl)cyclohexyl methylsulfonate

Chemical Property:

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Technology Process of (1R,2S,3S,6R)-2-hydroxy-6-methyl-3-(methylethyl)cyclohexyl methylsulfonate

There total 3 articles about (1R,2S,3S,6R)-2-hydroxy-6-methyl-3-(methylethyl)cyclohexyl methylsulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 308239-16-9
(1S,2R,3R,6S)-3-methyl-6-(methylethyl)-2-(methylsulfonyloxy)cyclohexyl benzoate

: 308239-17-0
(1R,2S,3S,6R)-2-hydroxy-6-methyl-3-(methylethyl)cyclohexyl methylsulfonate

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 7h;
DOI:10.1248/cpb.48.1536

Reference yield:

: 155419-08-2
(3S,6R)-3-Isopropyl-6-methyl-cyclohexane-1,2-diol

: 308239-17-0
(1R,2S,3S,6R)-2-hydroxy-6-methyl-3-(methylethyl)cyclohexyl methylsulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 6 h / 20 °C

2: 67 percent / pyridine; DMAP / CH₂Cl₂ / 48 h / Heating

3: 99 percent / K₂CO₃ / methanol / 7 h / 20 °C

With pyridine; dmap; potassium carbonate; In methanol; dichloromethane;
DOI:10.1248/cpb.48.1536

Reference yield:

: 308239-15-8
(1S,2R,3R,6S)-2-hydroxy-3-methyl-6-(methylethyl)cyclohexyl benzoate

: 308239-17-0
(1R,2S,3S,6R)-2-hydroxy-6-methyl-3-(methylethyl)cyclohexyl methylsulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / pyridine; DMAP / CH₂Cl₂ / 48 h / Heating

2: 99 percent / K₂CO₃ / methanol / 7 h / 20 °C

With pyridine; dmap; potassium carbonate; In methanol; dichloromethane;
DOI:10.1248/cpb.48.1536