(1S,2R,3R,6S)-3-methyl-6-(methylethyl)-2-(methylsulfonyloxy)cyclohexyl benzoate

Base Information

• Chemical Name: (1S,2R,3R,6S)-3-methyl-6-(methylethyl)-2-(methylsulfonyloxy)cyclohexyl benzoate
• CAS No.: 308239-16-9
• Molecular Formula: C₁₈H₂₆O₅S
• Molecular Weight: 354.467

Synonyms:(1S,2R,3R,6S)-3-methyl-6-(methylethyl)-2-(methylsulfonyloxy)cyclohexyl benzoate

Chemical Property of (1S,2R,3R,6S)-3-methyl-6-(methylethyl)-2-(methylsulfonyloxy)cyclohexyl benzoate

Chemical Property:

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Technology Process of (1S,2R,3R,6S)-3-methyl-6-(methylethyl)-2-(methylsulfonyloxy)cyclohexyl benzoate

There total 2 articles about (1S,2R,3R,6S)-3-methyl-6-(methylethyl)-2-(methylsulfonyloxy)cyclohexyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoyl chloride (98-88-4) → (1S,2R,3R,6S)-3-methyl-6-(methylethyl)-2-(methylsulfonyloxy)cyclohexyl benzoate (308239-16-9)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 6 h / 20 °C

2: 67 percent / pyridine; DMAP / CH₂Cl₂ / 48 h / Heating

With pyridine; dmap; In dichloromethane;

DOI:10.1248/cpb.48.1536

Reference yield:

(3S,6R)-3-Isopropyl-6-methyl-cyclohexane-1,2-diol (155419-08-2) → (1S,2R,3R,6S)-3-methyl-6-(methylethyl)-2-(methylsulfonyloxy)cyclohexyl benzoate (308239-16-9)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 6 h / 20 °C

2: 67 percent / pyridine; DMAP / CH₂Cl₂ / 48 h / Heating

With pyridine; dmap; In dichloromethane;

DOI:10.1248/cpb.48.1536

Reference yield: 99.0%

(1S,2R,3R,6S)-3-methyl-6-(methylethyl)-2-(methylsulfonyloxy)cyclohexyl benzoate (308239-16-9) → (1R,2S,3S,6R)-2-hydroxy-6-methyl-3-(methylethyl)cyclohexyl methylsulfonate (308239-17-0)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 7h;

DOI:10.1248/cpb.48.1536

upstream raw materials:

benzoyl chloride

(3S,6R)-3-Isopropyl-6-methyl-cyclohexane-1,2-diol

Downstream raw materials:

(1R,2S,3S,6R)-2-hydroxy-6-methyl-3-(methylethyl)cyclohexyl methylsulfonate

(1S,2S,3R,6S)-3-methyl-6-(methylethyl)cyclohexane-1,2-diol

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