1H-1,2,4-Triazole, 1-acetyl-2,5-dihydro-3-methoxy-5,5-dimethyl- (9CI)

Base Information

Chemical Name:1H-1,2,4-Triazole, 1-acetyl-2,5-dihydro-3-methoxy-5,5-dimethyl- (9CI)
CAS No.:118807-32-2
Molecular Formula:C₇H₁₃N₃O₂
Molecular Weight:171.199
Hs Code.:
Mol file:118807-32-2.mol

Synonyms:1H-1,2,4-Triazole,1-acetyl-2,5-dihydro-3-methoxy-5,5-dimethyl- (9CI)

Suppliers and Price of 1H-1,2,4-Triazole, 1-acetyl-2,5-dihydro-3-methoxy-5,5-dimethyl- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-1,2,4-Triazole, 1-acetyl-2,5-dihydro-3-methoxy-5,5-dimethyl- (9CI)

Chemical Property:

Melting Point:145-146 °C(Solv: ethyl ether (60-29-7))
Boiling Point:199.1±23.0 °C(Predicted)
PKA:3.41±0.40(Predicted)
PSA：53.93000
Density:1.20±0.1 g/cm3(Predicted)
LogP:-0.20610

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-1,2,4-Triazole, 1-acetyl-2,5-dihydro-3-methoxy-5,5-dimethyl- (9CI)

There total 3 articles about 1H-1,2,4-Triazole, 1-acetyl-2,5-dihydro-3-methoxy-5,5-dimethyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 118807-27-5
1,4-diacetyl-5,5-dimethyl-3-methylsulfonyl-4,5-dihydro-1H-1,2,4-triazole

: 118807-32-2
1-(3-Methoxy-5,5-dimethyl-4,5-dihydro-[1,2,4]triazol-1-yl)-ethanone

: 118807-33-3
1-(3-Methanesulfonyl-5,5-dimethyl-4,5-dihydro-[1,2,4]triazol-1-yl)-ethanone

Guidance literature:: With methanol; sodium methylate; for 0.25h; Ambient temperature;

Reference yield: 19.0%

: 124-41-4
sodium methylate

: 118807-27-5
1,4-diacetyl-5,5-dimethyl-3-methylsulfonyl-4,5-dihydro-1H-1,2,4-triazole

: 118807-32-2
1-(3-Methoxy-5,5-dimethyl-4,5-dihydro-[1,2,4]triazol-1-yl)-ethanone

: 118807-33-3
1-(3-Methanesulfonyl-5,5-dimethyl-4,5-dihydro-[1,2,4]triazol-1-yl)-ethanone

Guidance literature:: With methanol; for 0.25h; Ambient temperature;

Reference yield:

: 118807-35-5
1,4-diacetyl-5,5-dimethyl-3-methylthio-4,5-dihydro-1H-1,2,4-triazole

: 118807-32-2
1-(3-Methoxy-5,5-dimethyl-4,5-dihydro-[1,2,4]triazol-1-yl)-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 80 percent m-CPBA / CHCl₃ / 3 h / Ambient temperature; 2 eq. reagent

2: 73 percent / MeOH / 0.25 h / Ambient temperature

With methanol; 3-chloro-benzenecarboperoxoic acid; In chloroform;