3-BENZYL-2-OXO-2,3-DIHYDRO-BENZOIMIDAZOLE-1-CARBOXYLIC ACID ETHYL ESTER

Base Information

Chemical Name:3-BENZYL-2-OXO-2,3-DIHYDRO-BENZOIMIDAZOLE-1-CARBOXYLIC ACID ETHYL ESTER
CAS No.:161468-70-8
Molecular Formula:C₁₇H₁₆N₂O₃
Molecular Weight:296.326
Hs Code.:
Mol file:161468-70-8.mol

Synonyms:Ethyl 2,3-dihydro-2-oxo-3-(phenylmethyl)-1H-benzimidazole-1-carboxylate

Suppliers and Price of 3-BENZYL-2-OXO-2,3-DIHYDRO-BENZOIMIDAZOLE-1-CARBOXYLIC ACID ETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
ETHYL 3-BENZYL-2-OXO-2,3-DIHYDRO-1H-1,3-BENZIMIDAZOLE-1-CARBOXYLATE 95.00%
5MG
$ 687.35

American Custom Chemicals Corporation
ETHYL 3-BENZYL-2-OXO-2,3-DIHYDRO-1H-1,3-BENZIMIDAZOLE-1-CARBOXYLATE 95.00%
10MG
$ 679.14

American Custom Chemicals Corporation
ETHYL 3-BENZYL-2-OXO-2,3-DIHYDRO-1H-1,3-BENZIMIDAZOLE-1-CARBOXYLATE 95.00%
1MG
$ 647.61

Total 3 raw suppliers

Chemical Property of 3-BENZYL-2-OXO-2,3-DIHYDRO-BENZOIMIDAZOLE-1-CARBOXYLIC ACID ETHYL ESTER

Chemical Property:

Boiling Point:441.8±38.0 °C(Predicted)
PKA:0.05±0.20(Predicted)
Density:1.290±0.06 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

ETHYL 3-BENZYL-2-OXO-2,3-DIHYDRO-1H-1,3-BENZIMIDAZOLE-1-CARBOXYLATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-BENZYL-2-OXO-2,3-DIHYDRO-BENZOIMIDAZOLE-1-CARBOXYLIC ACID ETHYL ESTER

There total 3 articles about 3-BENZYL-2-OXO-2,3-DIHYDRO-BENZOIMIDAZOLE-1-CARBOXYLIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 41120-23-4
ethyl 2-oxo-2,3-dihydro-1H-benzo[d]imidazole-1-carboxylate

: 100-51-6,185532-71-2
benzyl alcohol

: 161468-70-8
Ethyl 2,3-dihydro-2-oxo-3-(phenylmethyl)-1H-benzimidazole-1-carboxylate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jo00111a014

Reference yield: 91.0%

: 41120-23-4
ethyl 2-oxo-2,3-dihydro-1H-benzo[d]imidazole-1-carboxylate

: 100-39-0
benzyl bromide

: 161468-70-8
Ethyl 2,3-dihydro-2-oxo-3-(phenylmethyl)-1H-benzimidazole-1-carboxylate

Guidance literature:: With potassium carbonate; In acetonitrile; Heating;
DOI:10.1021/jo00111a014

Reference yield:

: 615-16-7
1,3-dihydro-2H-benzimidazol-2-one

: 161468-70-8
Ethyl 2,3-dihydro-2-oxo-3-(phenylmethyl)-1H-benzimidazole-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / K₂CO₃ / acetonitrile / 0.5 h / Heating

2: 91 percent / K₂CO₂ / acetonitrile / Heating

With potassium carbonate; In acetonitrile;
DOI:10.1021/jo00111a014