dimethyl 2-cyclohexylidenesuccinate

Base Information

Chemical Name:dimethyl 2-cyclohexylidenesuccinate
CAS No.:40745-21-9
Molecular Formula:C₁₂H₁₈O₄
Molecular Weight:226.273
Hs Code.:

Synonyms:dimethyl 2-cyclohexylidenesuccinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl 2-cyclohexylidenesuccinate

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Technology Process of dimethyl 2-cyclohexylidenesuccinate

There total 8 articles about dimethyl 2-cyclohexylidenesuccinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 624-48-6
dimethyl cis-but-2-ene-1,4-dioate

: 1122-60-7
1-nitrocyclohexane

: 40745-21-9
dimethyl 2-cyclohexylidenesuccinate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 25 ℃; for 7h;
DOI:10.1016/S0040-4020(99)00829-7

Reference yield: 80.0%

: 624-49-7
dimethylfumarate

: 1122-60-7
1-nitrocyclohexane

: 40745-21-9
dimethyl 2-cyclohexylidenesuccinate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1002/1099-0690(200008)2000:16<2927::aid-ejoc2927>3.3.co;2-p

Reference yield: 60.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 106-65-0
Dimethyl succinate

: 40745-21-9
dimethyl 2-cyclohexylidenesuccinate

Guidance literature:: Dimethyl succinate; With potassium tert-butylate; In tert-butyl alcohol; Inert atmosphere;

cyclohexanone; In tert-butyl alcohol; at 25 ℃; Inert atmosphere;

With sulfuric acid; In methanol; for 8h; Reflux;
DOI:10.1055/s-0029-1219233