2-[(6,7-difluoro-2-phenylquinazolin-4-ylidene)hydrazonomethyl]-6-nitrophenyloxidozinc(II) acetate

Base Information

Chemical Name:2-[(6,7-difluoro-2-phenylquinazolin-4-ylidene)hydrazonomethyl]-6-nitrophenyloxidozinc(II) acetate
CAS No.:1394844-83-7
Molecular Formula:C₂₃H₁₅F₂N₅O₅Zn
Molecular Weight:544.789
Hs Code.:

Synonyms:2-[(6,7-difluoro-2-phenylquinazolin-4-ylidene)hydrazonomethyl]-6-nitrophenyloxidozinc(II) acetate

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Chemical Property of 2-[(6,7-difluoro-2-phenylquinazolin-4-ylidene)hydrazonomethyl]-6-nitrophenyloxidozinc(II) acetate

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Technology Process of 2-[(6,7-difluoro-2-phenylquinazolin-4-ylidene)hydrazonomethyl]-6-nitrophenyloxidozinc(II) acetate

There total 4 articles about 2-[(6,7-difluoro-2-phenylquinazolin-4-ylidene)hydrazonomethyl]-6-nitrophenyloxidozinc(II) acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1394844-75-7
N-(6,7-difluoro-2-phenylquinazolin-4-yl)-N'-(5-nitrosalicylidene)hydrazine

: 557-34-6
zinc diacetate

: 1394844-83-7
2-[(6,7-difluoro-2-phenylquinazolin-4-ylidene)hydrazonomethyl]-6-nitrophenyloxidozinc(II) acetate

Guidance literature:: With potassium hydroxide; In methanol; at 20 ℃; for 48h;
DOI:10.1007/s11172-011-0360-z

Reference yield:

: 6,7-difluoro-2-phenylquinazolin-4(3H)-one

: 1394844-83-7
2-[(6,7-difluoro-2-phenylquinazolin-4-ylidene)hydrazonomethyl]-6-nitrophenyloxidozinc(II) acetate

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / 1.5 h / Reflux

2: hydrazine hydrate / ethanol / 3 h / 70 °C

3: ethanol / 1.5 h / Reflux

4: potassium hydroxide / methanol / 48 h / 20 °C

With hydrazine hydrate; potassium hydroxide; trichlorophosphate; In methanol; ethanol;
DOI:10.1007/s11172-011-0360-z

Reference yield:

: 1394844-68-8
6,7-difluoro-4-hydrazino-2-phenylquinazoline

: 1394844-83-7
2-[(6,7-difluoro-2-phenylquinazolin-4-ylidene)hydrazonomethyl]-6-nitrophenyloxidozinc(II) acetate

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 1.5 h / Reflux

2: potassium hydroxide / methanol / 48 h / 20 °C

With potassium hydroxide; In methanol; ethanol;
DOI:10.1007/s11172-011-0360-z